FACILE SYNTHESIS OF 1,5-BENZOTHIAZEPINES IN WATER USING TETRABUTYLAMMONIUM TRIBROMIDE

被引：8
|
作者：
Yan, Yunhui [2 ]
Yang, Xiaojuan [3 ]
Wu, Liqiang [1 ]
机构：
[1] Xinxiang Med Univ, Sch Pharm, Xinxiang 453003, Henan, Peoples R China
[2] Xinxiang Med Univ, Sch Basic Med, Xinxiang 453003, Henan, Peoples R China
[3] Xinxiang Univ, Coll Chem & Chem Engn, Xinxiang, Henan, Peoples R China
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2012年 / 187卷 / 05期
关键词：
1,5-Benzothiazepines; 2-aminothiophenol; 1,3-diaryl-2-propenones; tetrabutylammonium tribromide; THIA-MICHAEL ADDITION; HIGHLY EFFICIENT; ALPHA; BETA-UNSATURATED KETONES; CARBONYL-COMPOUNDS; CATALYST; 1,5-BENZODIAZEPINES; BENZOTHIAZEPINE; DERIVATIVES; CLEAVAGE; SOLVENT;
D O I：
10.1080/10426507.2011.627900
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A simple, environmentally benign, and efficient method was developed for the preparation of 1,5-benzothiazepines via a one-pot condensation reaction of 2-aminothiophenol with 1,3-diaryl- 2-propenones using tetrabutylammonium tribromide as an efficient and versatile catalyst in water.
引用
收藏
页码：573 / 579
页数：7
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