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Green Protocol for Synthesis of 1,5-Benzodiazepines and 1,5-Benzothiazepines in the Presence of Nanocrystalline Aluminum Oxide
被引:21
|作者:
Hekmatshoar, Rahim
[1
]
Sadjadi, Sodeh
[1
]
Shiri, Soudeh
[1
]
Heravi, Majid M.
[1
]
Beheshtiha, Yahya S.
[1
]
机构:
[1] Alzahra Univ, Sch Sci, Dept Chem, Tehran, Iran
关键词:
o-Aminothiophenol;
1;
5-benzodiazepine;
5-benzothiazepine;
nanocrystalline aluminum oxide;
o-phenylenediamines;
reusable catalyst;
RECYCLABLE CATALYSTS;
EFFICIENT SYNTHESIS;
DERIVATIVES;
HETEROPOLYACIDS;
TRIFLATE;
SOLVENT;
D O I:
10.1080/00397910802657925
中图分类号:
O62 [有机化学];
学科分类号:
070303 ;
081704 ;
摘要:
An efficient protocol associated with readily available starting materials, mild conditions, excellent yields, and a broad range of the products in synthetic chemistry was established for synthesis of 1,5-benzodiazepine and 1,5-benzothiazepine derivatives in the presence of a catalytic amount of nanocrystalline aluminum oxide in water.
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页码:2549 / 2559
页数:11
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