Mono and bis[N-aryl(benzyl)]amides of phosphorylacetic acids. One-pot synthesis and extraction of actinides from nitric acid solutions

被引：0
|
作者：
O. I. Artyushin
E. V. Sharova
I. L. Odinets
K. A. Lyssenko
D. G. Golovanov
T. A. Mastryukova
G. A. Pribylova
I. G. Tananaev
G. V. Myasoedova
机构：
[1] Russian Academy of Sciences,A. N. Nesmeyanov Institute of Organoelement Compounds
[2] Russian Academy of Sciences,V. I. Vernadsky Institute of Geochemistry and Analytical Chemistry
来源：
Russian Chemical Bulletin | 2006年 / 55卷
关键词：
aromatic amines; phenylenediamines; xylylenediamines; phosphorylacetic acids; phosphorylacetic acid amides; carbamoylmethylphosphine oxides; actinides, americium; extraction;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A one-pot synthetic route to phosphorylacetic acid N-aryl(alkylaryl)amides, including those containing two phosphorylmethylcarbamoyl moieties attached to the arene framework, has been developed. The method is based on reactions of amines with the corresponding acid chlorides generated in situ with the use of phosphorus trichloride as a mild chlorinating agent. The compositions and structures of the compounds obtained and their extraction ability toward AmIII were determined. Suggestions were made about the compositions of the extracted complexes with phosphorylacetic acid N-aryl(alkylaryl)amides.
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页码：1440 / 1447
页数：7
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