2,2-Bis(methoxy- and ethoxy-NNO-azoxy)propane-1,3-diol sulfonates

被引:0
|
作者
I. N. Zyuzin
机构
[1] Russian Academy of Sciences,Institute of Problems of Chemical Physics
来源
关键词
Diol; Colorless Crystal; Sulfonyl Chloride; Anhydrous Acetonitrile; Sulfonic Ester;
D O I
暂无
中图分类号
学科分类号
摘要
2,2-Bis(alkoxy-NNO-azoxy)propane-1,3-diols react with sulfonyl chlorides and trifluoromethanesulfonic anhydride in the presence of bases affording previously unknown methane-, trifluoromethane-, benzene and toluenesulfonates (sulfonic esters) of 2-bis(methoxy- and ethoxy-NNO-azoxy)propane-1,3-diols. The triflates are thermally less stable than mesylates, benzenesulfonates, and tosylates of the corresponding diols.
引用
收藏
页码:631 / 634
页数:3
相关论文
共 50 条
  • [1] 2,2-Bis(methoxy- and ethoxy-NNO-azoxy)propane-1,3-diol sulfonates
    Zyuzin, I. N.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2014, 50 (05) : 631 - 634
  • [2] Potential Energetic Plasticizers on the Basis of 2,2-Dinitropropane-1,3-diol and 2,2-Bis(azidomethyl)propane-1,3-diol
    Hafner, Sven
    Hartdegen, Vera A.
    Hofmayer, Maximilian S.
    Klapoetke, Thomas M.
    PROPELLANTS EXPLOSIVES PYROTECHNICS, 2016, 41 (05) : 806 - 813
  • [3] Polyurethanes based on 2,2-dinitropropane-1,3-diol and 2,2-bis(azidomethyl) propane-1,3-diol as potential energetic binders
    Bellan, Andreas B.
    Hafner, Sven
    Hartdegen, Vera A.
    Klapoetke, Thomas M.
    JOURNAL OF APPLIED POLYMER SCIENCE, 2016, 133 (40)
  • [4] 2,2′-(p-Phenylenedimethylene)bis(propane-1,3-diol)
    Gao, Yajun
    Xi, Haitao
    Sun, Xiaoqiang
    Fu, Yongsheng
    Liu, Li
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O170 - U2745
  • [5] The mixed diol-dithiol 2,2-bis(sulfanylmethyl)propane-1,3-diol: characterization of key intermediates on a new synthetic pathway
    Simmons, Trevor R.
    Pickett, Christopher J.
    Wright, Joseph A.
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2011, 67 : O1 - O5
  • [6] N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles
    Igor N. Zyuzin
    Kirill Yu. Suponitsky
    Igor L. Dalinger
    Chemistry of Heterocyclic Compounds, 2017, 53 : 702 - 709
  • [7] N-[2,2-Bis(methoxy-NNO-azoxy)ethyl]pyrazoles
    Zyuzin, Igor N.
    Suponitsky, Kirill Yu.
    Dalinger, Igor L.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2017, 53 (6-7) : 702 - 709
  • [8] Thermal Decomposition of 1-[2,2-Bis(Methoxy-NNO-Azoxy)Ethyl]-Pyrazole
    Zakharov, V. V.
    Zyuzin, I. N.
    Korsunskiy, B. L.
    Larikova, T. S.
    Chukanov, N., V
    RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B, 2022, 16 (06) : 1038 - 1043
  • [9] Thermal Decomposition of 1-[2,2-Bis(Methoxy-NNO-Azoxy)Ethyl]-Pyrazole
    V. V. Zakharov
    I. N. Zyuzin
    B. L. Korsunskiy
    T. S. Larikova
    N. V. Chukanov
    Russian Journal of Physical Chemistry B, 2022, 16 : 1038 - 1043
  • [10] A practical and efficient procedure for preparation of diacetals from 2,2-bis(hydroxymethyl)propane-1,3-diol with aldehydes and ketones catalysed by anhydrous ferrous sulfate
    Jin, TS
    Ma, YR
    Li, TS
    Wang, JX
    JOURNAL OF CHEMICAL RESEARCH-S, 1999, (04): : 268 - 269