Applications of adsorption microcalorimetry for the characterization of metal-based catalysts

被引：26
|
作者：
Spiewak, BE [1 ]
Dumesic, JA [1 ]
机构：
[1] Univ Wisconsin, Dept Chem Engn, Madison, WI 53706 USA
来源：
THERMOCHIMICA ACTA | 1998年 / 312卷 / 1-2期
基金：
美国国家科学基金会;
关键词：
adsorption; catalysts; microcalorimetry; powders; single crystals; thin films; transition metals;
D O I：
10.1016/S0040-6031(97)00443-7
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
Microcalorimetry is a useful tool for studies of heterogeneous catalysts, because it provides a direct measurement of the strength with which molecules interact with solid surfaces. The following communication reviews adsorption microcalorimetric studies of unsupported metals and metal-based catalysts performed over the last 20 years, and then presents three advanced microcalorimetric techniques and their applications to the study of low surface-area-metal single crystals, films and powders, and metal surfaces/catalysts that are highly reactive toward oxygenates. (C) 1998 Elsevier Science B.V.
引用
收藏
页码：95 / 104
页数：10
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