Unexpected formation of 1,4-diphenylbutylphosphinic acid from 1,4-diphenylbuta-1,3-diene and elemental phosphorus via the Trofimov-Gusarova reaction

被引：8
|
作者：
Artem'ev, Alexander V. [1 ]
Sutyrina, Anastasiya O. [2 ]
Matveeva, Elena A. [2 ]
Albanov, Alexander I. [2 ]
Klyba, Lyudmila V. [2 ]
机构：
[1] Russian Acad Sci, Siberian Branch, AV Nikolaev Inst Inorgan Chem, Novosibirsk 630090, Russia
[2] Russian Acad Sci, Siberian Branch, AE Favorsky Irkutsk Inst Chem, Irkutsk 664033, Russia
来源：
MENDELEEV COMMUNICATIONS | 2017年 / 27卷 / 02期
关键词：
WHITE PHOSPHORUS; FUNCTIONALIZATION; CHEMISTRY;
D O I：
10.1016/j.mencom.2017.03.009
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
trans,trans-1,4-Diphenylbuta-1,3-diene reacts with elemental (red) phosphorus in the superbasic KOH/DMSO (H2O) system (120 degrees C, 3 h) to give, after acidic work-up, 1,4-di-phenylbutylphosphinic acid in 48% yield.
引用
收藏
页码：137 / 138
页数：2
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