Structure of μ-oxo-bis{{2,2′-[propane-1,3-diylbis (aminomethyl)]diphenolato}oxorhenium(V)}

被引：2

作者：

Huang, WT ^{[1
]}

Yao, HH

Chen, BH

Liao, FL

Lo, JM

机构：

[1] Yuanpei Inst Sci & Technol, Dept Radiol Technol, Hsinchu, Taiwan

[2] Taiwan Salt Corp, Tainan, Taiwan

[3] Natl Tsing Hua Univ, Dept Chem, Hsinchu, Taiwan

[4] Natl Tsing Hua Univ, Dept Nucl Sci, Hsinchu, Taiwan

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2002年 / 32卷 / 11期

关键词：

oxorhenium(V); hexacoordinate; binuclear; octahedral coordination;

D O I：

10.1023/A:1021192725915

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C34H40N4O7Re2, each of the two Re(V) atoms is hexacoordinated by two amine nitrogens, two phenol oxygens, and two axial oxygens. The compound is a binuclear complex with an O=Re-O-Re=O backbone and nearly octahedral coordination geometry at each Re atom. The Re=O bond distance is 1.720(14) Angstrom and the Re-O bridge bond distance is 1.938(12) Angstrom. The equatorial plane Re-O bond distances are 1.992(14) and 2.012(13) Angstrom, whereas the Re-N bond distances are 2.129(15) and 2.187(16) Angstrom.

引用

页码：465 / 468

页数：4

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