Synthesis and Features of Crystal Structure of Scandium Hexa(isothiocyanato)chromate(III) Complex with Nicotinic Acid

被引：1

作者：

Cherkasova, E. V. ^{[1
]}

Pervukhina, N. V. ^{[2
]}

Kuratieva, N. V. ^{[2
,3
]}

Cherkasova, T. G. ^{[1
]}

机构：

[1] Kuzbass State Tech Univ, Kemerovo 650000, Russia

[2] Russian Acad Sci, Nikolaev Inst Inorgan Chem, Siberian Branch, Novosibirsk 630090, Russia

[3] Novosibirsk State Univ, Novosibirsk 630090, Russia

来源：

RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2018年 / 63卷 / 06期

关键词：

D O I：

10.1134/S0036023618060050

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A double complex compound with a polymeric cation of composition [Sc-2(C6H5NO2)(3)(C6H4NO2)(3)][Cr(NCS)(6)] has been synthesized by the reaction between Sc(NO3)(3), K-3[Cr(NCS)(6)], and nicotinic acid (C5H5NCOO) in an aqueous solution and studied by chemical analysis, IR spectroscopy, and X-ray diffraction. Crystals are hexagonal, space group P6(3)22, Z = 2; a = 12.995(2) , c = 17.864(3) , V = 2612.3(7) 3, rho(calc) = 1.559 g/cm(3).

引用

页码：776 / 780

页数：5

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