A simple and efficient hydrolyzing method for tetrahydropyranyl ethers

被引:29
|
作者
Lee, ASY [1 ]
Su, FY [1 ]
Liao, YC [1 ]
机构
[1] Tamkang Univ, Dept Chem, Tamsui 251, Taiwan
关键词
D O I
10.1016/S0040-4039(98)02602-1
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A series of tetrahydropyranyl ethers are hydrolyzed to the corresponding alcohols in a CBr4/CH3OH (5% / 5mL) reaction system under refluxing. This method also enables to deprotect other functionalities such as acetals and ketals. (C) 1999 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:1323 / 1326
页数:4
相关论文
共 50 条
  • [11] Efficient deprotection of tetrahydropyranyl ethers by silica sulfuric acid
    Hajipour, AR
    Zarei, A
    Khazdooz, L
    Pourmousavi, SA
    Zahmatkesh, S
    Ruoho, AE
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2006, 45 (01): : 305 - 308
  • [12] Efficient deprotection of tetrahydropyranyl ethers by bismuth(III) salts
    Mohammadpoor-Baltork, I
    Kharamesh, B
    Kolagar, S
    SYNTHETIC COMMUNICATIONS, 2002, 32 (11) : 1633 - 1637
  • [13] DDQ AS A MILD AND EFFICIENT CATALYST FOR DEPROTECTION OF TETRAHYDROPYRANYL ETHERS
    RAINA, S
    SINGH, VK
    SYNTHETIC COMMUNICATIONS, 1995, 25 (16) : 2395 - 2400
  • [14] Environmentally benign and simple protocol for synthesis and cleavage of tetrahydropyranyl ethers
    Bandgar, BP
    Kasture, SP
    Patil, SV
    Makone, SS
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2003, 13 (01) : 83 - 84
  • [15] Zinc triflate: A mild and efficient catalyst for deprotection of tetrahydropyranyl ethers
    Srinivasulu, R.
    Satyanarayana, P. V. V.
    Kumar, K. Ravi
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2013, 83 (12) : 2419 - 2422
  • [16] Bismuth triflate: An efficient catalyst for the formation and deprotection of tetrahydropyranyl ethers
    Stephens, JR
    Butler, PL
    Clow, CH
    Oswald, MC
    Smith, RC
    Mohan, RS
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2003, 2003 (19) : 3827 - 3831
  • [17] STEROID TETRAHYDROPYRANYL ETHERS
    DAUBEN, WG
    BRADLOW, HL
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1952, 74 (02) : 559 - 560
  • [18] Zinc triflate: A mild and efficient catalyst for deprotection of tetrahydropyranyl ethers
    R. Srinivasulu
    P. V. V. Satyanarayana
    K. Ravi Kumar
    Russian Journal of General Chemistry, 2013, 83 : 2419 - 2422
  • [19] An efficient method for selective deprotection of trimethylsilyl ethers, tetrahydropyranyl ethers, ethylene acetals and ketals under solvent-free conditions
    Hajipour, AR
    Mallakpour, SE
    Mohammadpoor-Baltork, I
    Khoee, S
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2002, 41 (06): : 1251 - 1256
  • [20] A mild and efficient method for the cleavage of tert-butyldimethylsilyl and tetrahydropyranyl ethers by ceric ammonium nitrate in methanol
    DattaGupta, A
    Singh, R
    Singh, VK
    SYNLETT, 1996, (01) : 69 - &