Efficient deprotection of tetrahydropyranyl ethers by silica sulfuric acid

被引：0
|
作者：
Hajipour, AR
Zarei, A
Khazdooz, L
Pourmousavi, SA
Zahmatkesh, S
Ruoho, AE
机构：
[1] Univ Wisconsin, Sch Med, Dept Pharmacol, Madison, WI 53706 USA
[2] Isfahan Univ Technol, Coll Chem, Pharmaceut Res Lab, Esfahan 84156, Iran
来源：
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 2006年 / 45卷 / 01期
关键词：
deprotection; tetrahydropyranyl ethers; silica sulfuric acid;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Treatment of tetrahydropyranyl (THP) ethers with silica sulfuric acid in methanol provides a simple and efficient process for deprotection of these ethers and the parent alcohols are obtained in excellent yields.
引用
收藏
页码：305 / 308
页数：4
相关论文
共 50 条
  • [1] DDQ AS A MILD AND EFFICIENT CATALYST FOR DEPROTECTION OF TETRAHYDROPYRANYL ETHERS
    RAINA, S
    SINGH, VK
    SYNTHETIC COMMUNICATIONS, 1995, 25 (16) : 2395 - 2400
  • [2] Efficient deprotection of tetrahydropyranyl ethers by bismuth(III) salts
    Mohammadpoor-Baltork, I
    Kharamesh, B
    Kolagar, S
    SYNTHETIC COMMUNICATIONS, 2002, 32 (11) : 1633 - 1637
  • [3] Simple and Efficient Method for Deprotection of Tetrahydropyranyl Ethers by Using Silica Supported Sodium Hydrogen Sulphate
    Kumar, K. Ravi
    Satyanarayana, P. V. V.
    Reddy, B. Srinivasa
    CHINESE JOURNAL OF CHEMISTRY, 2012, 30 (05) : 1189 - 1191
  • [4] Mild and efficient method for selective deprotection of tetrahydropyranyl ethers to alcohols
    Maiti, G
    Roy, SC
    JOURNAL OF ORGANIC CHEMISTRY, 1996, 61 (17): : 6038 - 6039
  • [5] Zinc triflate: A mild and efficient catalyst for deprotection of tetrahydropyranyl ethers
    Srinivasulu, R.
    Satyanarayana, P. V. V.
    Kumar, K. Ravi
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2013, 83 (12) : 2419 - 2422
  • [6] Bismuth triflate: An efficient catalyst for the formation and deprotection of tetrahydropyranyl ethers
    Stephens, JR
    Butler, PL
    Clow, CH
    Oswald, MC
    Smith, RC
    Mohan, RS
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2003, 2003 (19) : 3827 - 3831
  • [7] Zinc triflate: A mild and efficient catalyst for deprotection of tetrahydropyranyl ethers
    R. Srinivasulu
    P. V. V. Satyanarayana
    K. Ravi Kumar
    Russian Journal of General Chemistry, 2013, 83 : 2419 - 2422
  • [8] A simple and efficient procedure for deprotection of tetrahydropyranyl ethers catalysed by expansive graphite
    Zhang, ZH
    Li, TS
    Jin, TS
    Wang, JX
    JOURNAL OF CHEMICAL RESEARCH-S, 1998, (03): : 152 - 153
  • [9] The use of silica sulfuric acid as an efficient catalyst for deprotection of trimethylsilyl ethers to the corresponding alcohols under mild and heterogeneous conditions
    Bamoniri, A.
    Zolfigol, M. A.
    Mohammadpoor-Baltork, I.
    Mirjalili, B. F.
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2006, 3 (01) : 85 - 88
  • [10] The use of silica sulfuric acid as an efficient catalyst for deprotection of trimethylsilyl ethers to the corresponding alcohols under mild and heterogeneous conditions
    A. Bamoniri
    M. A. Zolfigol
    I. Mohammadpoor-Baltork
    B. F. Mirjalili
    Journal of the Iranian Chemical Society, 2006, 3 : 85 - 88
12345