Determination of Lignin Content in Plant Materials Using Solid-State 13C NMR Spectroscopy

被引：9
|
作者：
Kostryukov, S. G. [1 ]
Petrov, P. S. [1 ]
Kalyazin, V. A. [1 ]
Masterova, Yu. Yu. [1 ]
Tezikova, V. S. [1 ]
Khluchina, N. A. [1 ]
Labzina, L. Ya. [1 ]
Alalvan, D. Kh. [1 ]
机构：
[1] Natl Res Mordovian State Univ, Saransk 430005, Russia
来源：
POLYMER SCIENCE SERIES B | 2021年 / 63卷 / 05期
关键词：
LIGNOCELLULOSIC BIOMASS; CROSS-POLARIZATION; SUGARCANE BAGASSE; WOOD; PRETREATMENT; EXTRACTION; CONVERSION;
D O I：
10.1134/S1560090421050067
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
The article shows the possibilities of solid-state (CP MAS) C-13 NMR spectroscopy for determination of lignin content in a wide range of lignocellulosic materials: wood of various tree species and plant waste. The analysis is based on the use of the dependences of the integral intensity of C-13 NMR signals due to aromatic or methoxy carbon atoms of lignin on its percentage in mixtures with cellulose. The lignin content obtained by C-13 NMR spectroscopy is in good agreement with the published data and the results obtained using acid hydrolysis of the corresponding samples of lignocellulosic biomaterials.
引用
收藏
页码：544 / 552
页数：9
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