Determination of Lignin Content in Plant Materials Using Solid-State 13C NMR Spectroscopy

被引：9
|
作者：
Kostryukov, S. G. [1 ]
Petrov, P. S. [1 ]
Kalyazin, V. A. [1 ]
Masterova, Yu. Yu. [1 ]
Tezikova, V. S. [1 ]
Khluchina, N. A. [1 ]
Labzina, L. Ya. [1 ]
Alalvan, D. Kh. [1 ]
机构：
[1] Natl Res Mordovian State Univ, Saransk 430005, Russia
来源：
POLYMER SCIENCE SERIES B | 2021年 / 63卷 / 05期
关键词：
LIGNOCELLULOSIC BIOMASS; CROSS-POLARIZATION; SUGARCANE BAGASSE; WOOD; PRETREATMENT; EXTRACTION; CONVERSION;
D O I：
10.1134/S1560090421050067
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
The article shows the possibilities of solid-state (CP MAS) C-13 NMR spectroscopy for determination of lignin content in a wide range of lignocellulosic materials: wood of various tree species and plant waste. The analysis is based on the use of the dependences of the integral intensity of C-13 NMR signals due to aromatic or methoxy carbon atoms of lignin on its percentage in mixtures with cellulose. The lignin content obtained by C-13 NMR spectroscopy is in good agreement with the published data and the results obtained using acid hydrolysis of the corresponding samples of lignocellulosic biomaterials.
引用
收藏
页码：544 / 552
页数：9
相关论文
共 50 条
  • [31] Structural Identification of Polyacrylonitrile during Thermal Treatment by Selective 13C Labeling and Solid-State 13C NMR Spectroscopy
    Wang, Yusong
    Xu, Lianghua
    Wang, Mozhen
    Pang, Wenmin
    Ge, Xuewu
    MACROMOLECULES, 2014, 47 (12) : 3901 - 3908
  • [32] Solid-state photodimerization of 9-methylanthracene as studied by solid-state 13C NMR
    Takegoshi, K
    Nakamura, S
    Terao, T
    SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1998, 11 (3-4) : 189 - 196
  • [33] Investigation of zeolitic imidazolate frameworks using 13C and 15N solid-state NMR spectroscopy
    Sneddon, Scott
    Kahr, Jurgen
    Orsi, Angelica F.
    Price, David J.
    Dawson, Daniel M.
    Wright, Paul A.
    Ashbrook, Sharon E.
    SOLID STATE NUCLEAR MAGNETIC RESONANCE, 2017, 87 : 54 - 64
  • [34] Contributors and potential of hydrocarbon generation of source rocks by solid-state 13C NMR spectroscopy
    WANGZhaoyun
    ChineseScienceBulletin, 1997, (06) : 478 - 481
  • [35] A straightforward detection of deprotonated conformers of malonic acid by solid-state 13C NMR spectroscopy
    Colsenet, R
    Gardiennet, C
    Henry, B
    Tekely, P
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2002, 41 (24) : 4743 - 4745
  • [36] Assessment of historic Tilia codrata wood by solid-state 13C CPMAS NMR spectroscopy
    Popescu, Carmen-Mihaela
    Demco, Dan E.
    Moeller, Martin
    POLYMER DEGRADATION AND STABILITY, 2013, 98 (12) : 2730 - 2734
  • [37] Analyzing the effects of thermal stress on insulator papers by solid-state 13C NMR spectroscopy
    Jusner, Paul
    Bacher, Markus
    Simon, Jonas
    Bausch, Florian
    Khaliliyan, Hajar
    Schiehser, Sonja
    Sumerskii, Ivan
    Schwaiger, Elisabeth
    Potthast, Antje
    Rosenau, Thomas
    CELLULOSE, 2022, 29 (02) : 1081 - 1095
  • [38] Characterization of bifunctional interpenetrating polymer networks via solid-state 13C NMR spectroscopy
    Crick, Darell W., 1600, (26):
  • [39] Analyzing the effects of thermal stress on insulator papers by solid-state 13C NMR spectroscopy
    Paul Jusner
    Markus Bacher
    Jonas Simon
    Florian Bausch
    Hajar Khaliliyan
    Sonja Schiehser
    Ivan Sumerskii
    Elisabeth Schwaiger
    Antje Potthast
    Thomas Rosenau
    Cellulose, 2022, 29 : 1081 - 1095
  • [40] Structural and dynamic study of chemically modified polyHIPE by solid-state 13C NMR spectroscopy
    Mercier, A
    Kuroki, S
    Ando, I
    Deleuze, H
    Mondain-Monval, O
    JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 2001, 39 (09) : 956 - 963
12345