Bis{2-[3-(2-pyridyl)pyrazol-1-ylmethyl]pyridine}-nickel(II) bis(perchlorate) chloroform disolvate

被引：4
|
作者：
Song, RF [1 ]
Li, JR
Zou, RQ
机构：
[1] Univ Sci Technol Suzhou, Dept Chem & Chem Engn, Suzhou 215009, Peoples R China
[2] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词：
D O I：
10.1107/S1600536805032046
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [Ni(C14H12N4)(2)](ClO4)(2)(.)2CHCl(3), each of the two crystallographically independent nickel(II) complex molecules lies on a twofold axis. In each case, the Ni II atom is coordinated by the six N atoms of two 2-[3-(2-pyridyl) pyrazol-1-ylmethyl] pyridine ligands in a distorted octahedral geometry. The Ni-N-pyrazole bond lengths [1.977 (3)-1.997 (4) angstrom] are appreciably shorter than the Ni-N-pyridine bond lengths [2.133 (4)-2.184 (4) angstrom].
引用
收藏
页码：M2305 / M2307
页数：3
相关论文
共 50 条
  • [41] 3-[3-(2-Pyridyl)-1H-pyrazol-1-yl]propanamide
    Huang, Feng
    Jin, Bin
    Zhang, Jian-Feng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01411 - U3038
  • [42] Bis(2,2′-bipyridine)[2-(2-pyridyl)-1H-benzimidazol-1-yl]ruthenium(II) perchlorate acetonitrile solvate monohydrate
    Liu, YJ
    Chao, H
    Yu, HJ
    Yuan, YX
    Ji, LN
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M585 - M587
  • [43] Bis[μ-3{5}-(2-pyridyl)pyrazolido]-bis[(acetonitrile)copper(II)] diperchlorate
    Hallam, MJ
    Kilner, CA
    Halcrow, MA
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2002, 58 (08): : m445 - m446
  • [44] Poly[[bis(acetonitrile-κN)bis{μ-2-[(2-carboxylatoethyl)ammoniomethyl] benzoato}copper(II)]bis(perchlorate) acetonitrile disolvate]
    Musie, Ghezai T.
    Li, Xiaobao
    Klausmeyer, Kevin K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : M1966 - M1968
  • [45] [1,4-bis(pyridyl-2-ylmethyl)-1,4-diazacycloheptane]-chlorocobalt(II) perchlorate
    Guo, YM
    Du, M
    Chen, ST
    Bu, XH
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 : M454 - M456
  • [46] Preparation and characterisation of rhenium(I) and platinum(IV) complexes of 2,6-bis(pyrazol-1-ylmethyl)pyridine and 2,6-bis(3,5-dimethylpyrazol-1-ylmethyl)pyridine. Crystal structure of fac-[ReI(CO)(3)(BMPz)]
    Orrell, KG
    Osborne, AG
    daSilva, MW
    Hursthouse, MB
    Coles, SJ
    POLYHEDRON, 1997, 16 (17) : 3003 - 3012
  • [47] {N-[Bis(2-pyridyl)methyl]-N,N-bis(2-pyridyl)methylamine-κ5N}chlorozinc(II) perchlorate monohydrate
    Kojima, T
    Weber, DM
    Choma, CT
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : M1291 - M1292
  • [48] N,N′-Bis[2-(2-pyridyl)ethyl]dithiooxamide
    Cui, JZ
    Zhang, D
    Pan, SW
    Cheng, P
    Liao, DZ
    Wang, GL
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1913 - O1915
  • [49] Synthesis and crystal structure of 2,3-bis[3-(2-pyridyl)pyrazol-1-yl]hydroquinone dihydrate at 158 K
    Hagback, PH
    Steel, PJ
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2001, 216 (01): : 60 - 62
  • [50] STRUCTURE OF BIS(N-[2-(2-PYRIDYL)ETHYL]-3-ETHOXYSALICYLIDENEAMINATO)COPPER(II)
    CASTINEIRAS, A
    HILLER, W
    STRAHLE, J
    ROMERO, J
    BASTIDA, R
    SOUSA, A
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1990, 46 : 770 - 772
12345