Bis{2-[3-(2-pyridyl)pyrazol-1-ylmethyl]pyridine}-nickel(II) bis(perchlorate) chloroform disolvate

被引：4
|
作者：
Song, RF [1 ]
Li, JR
Zou, RQ
机构：
[1] Univ Sci Technol Suzhou, Dept Chem & Chem Engn, Suzhou 215009, Peoples R China
[2] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词：
D O I：
10.1107/S1600536805032046
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [Ni(C14H12N4)(2)](ClO4)(2)(.)2CHCl(3), each of the two crystallographically independent nickel(II) complex molecules lies on a twofold axis. In each case, the Ni II atom is coordinated by the six N atoms of two 2-[3-(2-pyridyl) pyrazol-1-ylmethyl] pyridine ligands in a distorted octahedral geometry. The Ni-N-pyrazole bond lengths [1.977 (3)-1.997 (4) angstrom] are appreciably shorter than the Ni-N-pyridine bond lengths [2.133 (4)-2.184 (4) angstrom].
引用
收藏
页码：M2305 / M2307
页数：3
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