Comparative extraction of polychlorinated dibenzo-p-dioxins and dibenzofurans (PCDD/F-s) from a variety of solid samples

被引:0
|
作者
Wu, WZ [1 ]
Schramm, KW [1 ]
Henkelmann, B [1 ]
Xu, Y [1 ]
Zhang, YY [1 ]
Kettrup, A [1 ]
机构
[1] GSF FORSCHUNGSZENTRUM UMWELT & GESUNDHEIT,INST OKOL CHEM,D-85764 OBERSCHLEISSHEIM,GERMANY
关键词
PCDD/F-s; extraction; recovery;
D O I
暂无
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Extraction experiments with spiking of C-13(12)-PCDD/Fs were performed with a variety of PCDD/Fs contaminated samples. The extraction recovery of PCDD/Fs was mainly influenced by PCDD/Fs concentration and the sample matrix. Generally, the first soxhlet extraction with toluene has suitable recovery. From the selected samples, only FAMS4 and 5 which are fly ashes with high concentration, the recovery of the first soxhlet extraction with 24 hr. is low, but PCDD/Fs were almost completely removed after 72 hr. Copyright (C) 1996 Elsevier Science Ltd
引用
收藏
页码:2229 / 2237
页数:9
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