Construction of a hybrid clamped cell for high-pressure neutron-diffraction experiments with a large diamond window

被引：1

作者：

Benz, S. ^{[1
]}

Moeller, A. ^{[3
]}

Marioneck, T. ^{[1
]}

Hofmann, M. ^{[2
]}

Brenk, J. ^{[3
]}

Dronskowski, R. ^{[1
]}

机构：

[1] Rhein Westfal TH Aachen, Inst Inorgan Chem, Chair Solid State & Quantum Chem, D-52056 Aachen, Germany

[2] Tech Univ Munich, Res Neutron Source Heinz Maier Leibnitz FRM II, D-85748 Garching, Germany

[3] Rhein Westfal TH Aachen, Inst IME Proc Met & Met Recycling, D-52056 Aachen, Germany

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 2019年 / 90卷 / 02期

关键词：

DESIGN;

D O I：

10.1063/1.5066365

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

A hybrid pressure cell was fabricated from commercially available copper-beryllium and custom-made Ni-Cr-Al Russian alloy, tailored for usage as a reaction vessel supplying a volume of about 400 mm(3). In order to directly (in situ) monitor pressure and chemical reactions within the chamber, a large diamond window suitable for spectroscopic sample analysis was implemented. The performance of the hybrid cell was validated from high-pressure neutron-diffraction measurements on carbon dioxide. Published under license by AIP Publishing.

引用

页数：3

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