Construction of a hybrid clamped cell for high-pressure neutron-diffraction experiments with a large diamond window

被引：1
|
作者：
Benz, S. [1 ]
Moeller, A. [3 ]
Marioneck, T. [1 ]
Hofmann, M. [2 ]
Brenk, J. [3 ]
Dronskowski, R. [1 ]
机构：
[1] Rhein Westfal TH Aachen, Inst Inorgan Chem, Chair Solid State & Quantum Chem, D-52056 Aachen, Germany
[2] Tech Univ Munich, Res Neutron Source Heinz Maier Leibnitz FRM II, D-85748 Garching, Germany
[3] Rhein Westfal TH Aachen, Inst IME Proc Met & Met Recycling, D-52056 Aachen, Germany
来源：
REVIEW OF SCIENTIFIC INSTRUMENTS | 2019年 / 90卷 / 02期
关键词：
DESIGN;
D O I：
10.1063/1.5066365
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
A hybrid pressure cell was fabricated from commercially available copper-beryllium and custom-made Ni-Cr-Al Russian alloy, tailored for usage as a reaction vessel supplying a volume of about 400 mm(3). In order to directly (in situ) monitor pressure and chemical reactions within the chamber, a large diamond window suitable for spectroscopic sample analysis was implemented. The performance of the hybrid cell was validated from high-pressure neutron-diffraction measurements on carbon dioxide. Published under license by AIP Publishing.
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页数：3
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