Electron Diffraction of 3D Molecular Crystals

被引：47
|
作者：
Saha, Ambarneil [1 ,2 ]
Nia, Shervin S. [1 ,2 ]
Rodriguez, Jose A. [1 ,2 ]
机构：
[1] Univ Calif Los Angeles, UCLA DOE Inst Genom & Prote, Los Angeles, CA 90095 USA
[2] Univ Calif Los Angeles, Dept Chem & Biochem, Los Angeles, CA 90095 USA
来源：
CHEMICAL REVIEWS | 2022年 / 122卷 / 17期
关键词：
ACTIVE PHARMACEUTICAL INGREDIENTS; INITIO STRUCTURE DETERMINATION; STRUCTURE-BASED INHIBITORS; X-RAY CRYSTALLOGRAPHY; RADIATION-DAMAGE; PHASE DETERMINATION; SCATTERING FACTORS; DYNAMICAL DIFFRACTION; PRECESSION TECHNIQUE; HYDROGEN POSITIONS;
D O I：
10.1021/acs.chemrev.1c00879
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Electron crystallography has a storied history which rivals that of its more established X-ray-enabled counterpart. Recent advances in data collection and analysis have sparked a renaissance in the field, opening a new chapter for this venerable technique. Burgeoning interest in electron crystallography has spawned innovative methods described by various interchangeable labels (3D ED, MicroED, cRED, etc.). This Review covers concepts and findings relevant to the practicing crystallographer, with an emphasis on experiments aimed at using electron diffraction to elucidate the atomic structure of three-dimensional molecular crystals.
引用
收藏
页码：13883 / 13914
页数：32
相关论文
共 50 条
  • [31] Atomic electron tomography: 3D structures without crystals
    Miao, Jianwei
    Ercius, Peter
    Billinge, Simon J. L.
    SCIENCE, 2016, 353 (6306)
  • [32] Electron 3D crystallography of protein crystals for visualization of charges
    Yonekura, Koji
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2017, 73 : C811 - C811
  • [33] Structure of molecular crystals solved by automated electron diffraction
    Gorelik, Tatiana
    Mugnaioli, Enrico
    Stewart, Andrew
    Matveeva, Galina
    Kolb, Ute
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2010, 66 : S66 - S66
  • [34] Electron diffraction and imaging of 3D nanocrystals of pharmaceuticals, peptides and proteins
    Abrahams, Jan Pieter
    van Genderent, Eric
    Nederlof, Igor
    Clabbers, Max
    Li, Yaowang
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2015, 71 : S103 - S103
  • [35] Crystal Structure of Indomethacin Polymorph δ Solved by 3D Electron Diffraction
    Lightowler, Molly
    Li, Shuting
    Ou, Xiao
    Zou, Xiaodong
    Lu, Ming
    Xu, Hongyi
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2021, 77 : C255 - C255
  • [36] Crystal structure of copper perchlorophthalocyanine analysed by 3D electron diffraction
    Gorelik, Tatiana E.
    Habermehl, Stefan
    Shubin, Aleksandr A.
    Gruene, Tim
    Yoshida, Kaname
    Oleynikov, Peter
    Kaiser, Ute
    Schmidt, Martin U.
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2021, 77 : 662 - 675
  • [37] 3D Electron diffraction for the discovery of new crystal forms of APIs
    Lanza, A. E.
    Potticary, J.
    Hall, C.
    Hamilton, V.
    Hall, S. R.
    Santiso-Quinones, G.
    Steinfeld, G.
    Hovestreydt, E.
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2021, 77 : C879 - C879
  • [38] Accurate structure refinement from 3D electron diffraction data
    Palatinus, L.
    Correa, C.
    Mouillard, G.
    Boullay, P.
    Jacob, D.
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2014, 70 : C374 - C374
  • [39] A NEW PRINCIPLE OF ORIENTATION DETERMINATION FOR 3D ELECTRON DIFFRACTION MICROSCOPY
    Liu, H. H.
    Poulsen, H. F.
    Schmidt, S.
    Sorensen, H. O.
    Godfrey, A.
    Huang, X.
    CHALLENGES IN MATERIALS SCIENCE AND POSSIBILITIES IN 3D AND 4D CHARACTERIZATION TECHNIQUES, 2010, : 311 - 316
  • [40] Structural Study of Organic Cocrystals Using 3D Electron Diffraction
    Agbemeh, V. E.
    Sonaglioni, D.
    Andrusenko, I.
    Husanu, E.
    Gemmi, M.
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2022, 78 : E635 - E635
12345