Electron Diffraction of 3D Molecular Crystals

被引:47
|
作者
Saha, Ambarneil [1 ,2 ]
Nia, Shervin S. [1 ,2 ]
Rodriguez, Jose A. [1 ,2 ]
机构
[1] Univ Calif Los Angeles, UCLA DOE Inst Genom & Prote, Los Angeles, CA 90095 USA
[2] Univ Calif Los Angeles, Dept Chem & Biochem, Los Angeles, CA 90095 USA
关键词
ACTIVE PHARMACEUTICAL INGREDIENTS; INITIO STRUCTURE DETERMINATION; STRUCTURE-BASED INHIBITORS; X-RAY CRYSTALLOGRAPHY; RADIATION-DAMAGE; PHASE DETERMINATION; SCATTERING FACTORS; DYNAMICAL DIFFRACTION; PRECESSION TECHNIQUE; HYDROGEN POSITIONS;
D O I
10.1021/acs.chemrev.1c00879
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Electron crystallography has a storied history which rivals that of its more established X-ray-enabled counterpart. Recent advances in data collection and analysis have sparked a renaissance in the field, opening a new chapter for this venerable technique. Burgeoning interest in electron crystallography has spawned innovative methods described by various interchangeable labels (3D ED, MicroED, cRED, etc.). This Review covers concepts and findings relevant to the practicing crystallographer, with an emphasis on experiments aimed at using electron diffraction to elucidate the atomic structure of three-dimensional molecular crystals.
引用
收藏
页码:13883 / 13914
页数:32
相关论文
共 50 条
  • [21] Automated quantitative 3d electron diffraction rotation tomography
    Oleynikov, Peter
    Hovmoller, Sven
    Zou, Xiaodong
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2011, 67 : C175 - C176
  • [22] Biomolecular structure determination by electron diffraction of 3D microcrystals
    Nannenga, Brent
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2018, 74 : E5 - E5
  • [23] Ultrafast 3D imaging of isolated molecules with electron diffraction
    Yang, Jie
    Hensley, Christopher J.
    Centurion, Martin
    ULTRAFAST IMAGING AND SPECTROSCOPY, 2013, 8845
  • [24] Collecting 3D electron diffraction data by the rotation method
    Zhang, Daliang
    Oleynikov, Peter
    Hovmoller, Sven
    Zou, Xiaodong
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS, 2010, 225 (2-3): : 94 - 102
  • [25] The Crystal Structure of Orthocetamol Solved by 3D Electron Diffraction
    Andrusenko, Iryna
    Hamilton, Victoria
    Mugnaioli, Enrico
    Lanza, Arianna
    Hall, Charlie
    Potticary, Jason
    Hall, Simon R.
    Gemmi, Mauro
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2019, 58 (32) : 10919 - 10922
  • [26] Identifying almost identical phases by 3D electron diffraction
    Kodjikian, S.
    Klein, H.
    Lepoittevin, C.
    Darie, C.
    Bordet, P.
    Payen, C.
    Deudon, C.
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2014, 70 : C373 - C373
  • [27] DATA PROCESSING OF 3D PRECESSION ELECTRON DIFFRACTION DATA
    Palatinus, Lukas
    Brazda, Petr
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2019, 75 : E406 - E406
  • [28] Unraveling unforeseen disorders in silicates with 3D electron diffraction
    Cho, Jungyoun
    Zou, Xiaodong
    Willhammar, Tom
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2021, 77 : C1283 - C1283
  • [29] Quantitative 3D electron diffraction data by precession and electron rotation methods
    Hovmoller, Sven
    Oleynikov, Peter
    Sun, Junliang
    Zhang, Daliang
    Zou, Xiaodong
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : C76 - C76
  • [30] 3D diffraction imaging and orientation mapping in deformed ice crystals
    Donges, Jorn
    Montagnat, Maurine
    Bastie, Pierre
    Grennerat, Fanny
    NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2013, 300 : 6 - 10