Determination of Lead(II) Using Screen-Printed Bismuth-Antimony Film Electrode

被引：25
|
作者：
Chen, Chen [1 ]
Niu, Xiangheng [1 ]
Chai, Yan [1 ]
Zhao, Hongli [1 ]
Lan, Minbo [1 ,2 ]
Zhu, Yonggang [3 ,4 ]
Wei, Gang [5 ]
机构：
[1] E China Univ Sci & Technol, Shanghai Key Lab Funct Mat Chem, Shanghai 200237, Peoples R China
[2] E China Univ Sci & Technol, Minist Educ, Key Lab Ultrafine Mat, Shanghai 200237, Peoples R China
[3] CSIRO Mat Sci & Engn, Clayton, Vic 3169, Australia
[4] Melbourne Ctr Nanofabricat, Clayton, Vic 3168, Australia
[5] CSIRO Mat Sci & Engn, Lindfield, NSW 2070, Australia
来源：
ELECTROANALYSIS | 2013年 / 25卷 / 06期
关键词：
Bismuth-antimony film; Screen-printed electrodes; Stripping voltammetry; Lead(II) detection; ANODIC-STRIPPING VOLTAMMETRY; TRACE HEAVY-METALS; CARBON-PASTE ELECTRODE; ICP-AES; POWDER; IONS; CD; PB; SPECTROMETRY; BIOSENSORS;
D O I：
10.1002/elan.201200625
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
This work presents a disposable bismuth-antimony film electrode fabricated on screen-printed electrode (SPE) substrates for lead(II) determination. This bismuth-antimony film screen-printed electrode (Bi-SbSPE) is simply prepared by simultaneously in situ depositing bismuth(III) and antimony(III) with analytes on the homemade SPE. The Bi-SbSPE can provide an enhanced electrochemical stripping signal for lead(II) compared to bismuth film screen-printed electrodes (BiSPE), antimony film screen-printed electrodes (SbSPE) and bismuth-antimony film glassy carbon electrodes (Bi-SbGC). Under optimized conditions, the Bi-SbSPE exhibits attractive linear responses towards lead(II) with a detection limit of 0.07 mu g/L. The Bi-SbSPE has been demonstrated successfully to detect lead in river water sample.
引用
收藏
页码：1446 / 1452
页数：7
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