The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid

被引：0

作者：

Wang Liping ^{[1
]}

Deng Diandian ^{[1
]}

Yan Hewei ^{[1
]}

Sun Xiaoxia ^{[1
]}

Wei Chaochao ^{[1
]}

机构：

[1] Jiangxi Sci & Technol Normal Univ, Jiangxi Key Lab Organ Chem, Nanchang 330013, Peoples R China

来源：

PROCEEDINGS OF THE 2016 INTERNATIONAL FORUM ON ENERGY, ENVIRONMENT AND SUSTAINABLE DEVELOPMENT (IFEESD) | 2016年 / 75卷

关键词：

2,3-dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid; organic light-emmitting material; synthesis; pi-conjugated polymers; CONJUGATED POLYMERS; SELENOPHENE;

D O I：

暂无

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

A new synthetic approach to synthesize 2,3-dimethyl -2,3-dihydrofuro [3,4-b][1,4]dioxine-5,7 -dicarboxylic acid from a common precursor diglycolic acid was reported. Starting from the commercial material diethylene glycol, diethyl oxalate and 2,3-dibromobutane, the compound was synthesized through oxidation reaction, acylation, hydrolysis and elimination reaction with moderate yield via a five-step reaction. The procedure was described herein with several advantages, including high product yields and easy purification.

引用

页码：776 / 779

页数：4

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