The Synthesis of Novel Material 2,3-Dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid

被引：0
|
作者：
Wang Liping [1 ]
Deng Diandian [1 ]
Yan Hewei [1 ]
Sun Xiaoxia [1 ]
Wei Chaochao [1 ]
机构：
[1] Jiangxi Sci & Technol Normal Univ, Jiangxi Key Lab Organ Chem, Nanchang 330013, Peoples R China
来源：
PROCEEDINGS OF THE 2016 INTERNATIONAL FORUM ON ENERGY, ENVIRONMENT AND SUSTAINABLE DEVELOPMENT (IFEESD) | 2016年 / 75卷
关键词：
2,3-dimethyl-2,3-dihydrofuro[3,4-b][1,4]dioxine-5,7-dicarboxylic acid; organic light-emmitting material; synthesis; pi-conjugated polymers; CONJUGATED POLYMERS; SELENOPHENE;
D O I：
暂无
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
A new synthetic approach to synthesize 2,3-dimethyl -2,3-dihydrofuro [3,4-b][1,4]dioxine-5,7 -dicarboxylic acid from a common precursor diglycolic acid was reported. Starting from the commercial material diethylene glycol, diethyl oxalate and 2,3-dibromobutane, the compound was synthesized through oxidation reaction, acylation, hydrolysis and elimination reaction with moderate yield via a five-step reaction. The procedure was described herein with several advantages, including high product yields and easy purification.
引用
收藏
页码：776 / 779
页数：4
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