Preparation of organized Ti nanorods by successive electrochemical processes in aqueous solution and molten salt

被引：7

作者：

Yasuda, Kouji ^{[1
]}

Ghicov, Andrei ^{[2
]}

Nohira, Toshiyuki ^{[1
]}

Kani, Naoya ^{[1
]}

Hagiwara, Rika ^{[1
]}

Schmuki, Patrik ^{[2
]}

机构：

[1] Kyoto Univ, Dept Fundamental Energy Sci, Grad Sch Energy Sci, Kyoto 6068501, Japan

[2] Univ Erlangen Nurnberg, Dept Mat Sci, Inst Surface Sci & Corros LKO, D-91058 Erlangen, Germany

来源：

ELECTROCHEMICAL AND SOLID STATE LETTERS | 2008年 / 11卷 / 09期

关键词：

D O I：

10.1149/1.2943666

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

This paper reports on the preparation of organized Ti nanorods by a combination of two electrochemical processes: (i) an anodization of Ti metal in a fluoride-containing aqueous solution to produce self-organized TiO2 nanotubes, and (ii) a cathodic reduction of the TiO2 nanotubes in molten LiCl-KCl-CaCl2 at 773 K. The final product was confirmed to be basically organized metallic Ti nanorods with diameters around 100 nm by X-ray diffractometry, X-ray photoelectron spectroscopy, and field-emission scanning electron microscopy. (C) 2008 The Electrochemical Society.

引用

页码：C51 / C54

页数：4

共 50 条

[41] Preparation of Two-dimensional Ti2CTx by Molten Fluorinated Salt Method
Ming Yan
Lei Yang
Chao Li
Yunqi Zou
Journal of Wuhan University of Technology-Mater. Sci. Ed., 2019, 34 : 299 - 302
[42] Review of Recent Advances in Electrochemical Processes in Molten Salt Electrolyte for Recycling Used Nuclear Fuel
Choi, Eun-Young
Lee, Chang Hwa
KOREAN JOURNAL OF CHEMICAL ENGINEERING, 2024,
[43] Electrochemical behavior and dissolution processes of lithium metal in the LiCl–KCl–CsCl molten salt system
Chang, Shenyu
Zhu, Shigui
Lu, Guimin
Journal of Applied Electrochemistry, 2024,
[44] Preparation of α-Mno2 nanorods and Co3O4 submicrooctahedrons by molten salt route
Ran, Songlin
Gao, Lian
CHEMISTRY LETTERS, 2007, 36 (05) : 688 - 689
[45] Preparation and electrochemical studies of electrospun TiO2 nanofibers and molten salt method nanoparticles
Reddy, M. V.
Jose, R.
Teng, T. H.
Chowdari, B. V. R.
Ramakrishna, S.
ELECTROCHIMICA ACTA, 2010, 55 (09) : 3109 - 3117
[46] Preparation of γ-Uranium-Molybdenum Alloys by Electrochemical Reduction of Solid Oxides in LiCl Molten Salt
Zhong, Yu-Ke
Liu, Kui
Liu, Ya-Lan
Lu, Yue-Xiang
Yin, Tai-Qi
Wang, Lin
Chai, Zhi-fang
Shi, Wei-Qun
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2019, 166 (08) : D276 - D282
[47] Preparation of Al-Si Master Alloy by Electrochemical Reduction of Fly Ash in Molten Salt
Aimin Liu
Liangxing Li
Junli Xu
Zhongning Shi
Xianwei Hu
Bingliang Gao
Zhaowen Wang
Jiangyu Yu
Gong Chen
JOM, 2014, 66 : 694 - 699
[48] An electrochemical method for the preparation of Mg-Li alloys at low temperature molten salt system
Zhang, M. L.
Yan, Y. D.
Hou, Z. Y.
Fan, L. A.
Chen, Z.
Tang, D. X.
JOURNAL OF ALLOYS AND COMPOUNDS, 2007, 440 (1-2) : 362 - 366
[49] Preparation of Al-Si Master Alloy by Electrochemical Reduction of Fly Ash in Molten Salt
Liu, Aimin
Li, Liangxing
Xu, Junli
Shi, Zhongning
Hu, Xianwei
Gao, Bingliang
Wang, Zhaowen
Yu, Jiangyu
Chen, Gong
JOM, 2014, 66 (05) : 694 - 699
[50] In-situ synthesis of nanocrystalline TiC powders, nanorods, and nanosheets in molten salt by disproportionation reaction of Ti(II) species
Yang, Lingxu
Wang, Ying
Liu, Ruijia
Liu, Huijun
Zhang, Xue
Zeng, Chaoliu
Fu, Chao
JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY, 2020, 37 : 173 - 180

← 1 2 3 4 5 →