Preparation of organized Ti nanorods by successive electrochemical processes in aqueous solution and molten salt

被引：7
|
作者：
Yasuda, Kouji [1 ]
Ghicov, Andrei [2 ]
Nohira, Toshiyuki [1 ]
Kani, Naoya [1 ]
Hagiwara, Rika [1 ]
Schmuki, Patrik [2 ]
机构：
[1] Kyoto Univ, Dept Fundamental Energy Sci, Grad Sch Energy Sci, Kyoto 6068501, Japan
[2] Univ Erlangen Nurnberg, Dept Mat Sci, Inst Surface Sci & Corros LKO, D-91058 Erlangen, Germany
来源：
ELECTROCHEMICAL AND SOLID STATE LETTERS | 2008年 / 11卷 / 09期
关键词：
D O I：
10.1149/1.2943666
中图分类号：
O646 [电化学、电解、磁化学];
学科分类号：
081704 ;
摘要：
This paper reports on the preparation of organized Ti nanorods by a combination of two electrochemical processes: (i) an anodization of Ti metal in a fluoride-containing aqueous solution to produce self-organized TiO2 nanotubes, and (ii) a cathodic reduction of the TiO2 nanotubes in molten LiCl-KCl-CaCl2 at 773 K. The final product was confirmed to be basically organized metallic Ti nanorods with diameters around 100 nm by X-ray diffractometry, X-ray photoelectron spectroscopy, and field-emission scanning electron microscopy. (C) 2008 The Electrochemical Society.
引用
收藏
页码：C51 / C54
页数：4
相关论文
共 50 条
  • [21] Preparation and electrochemical lithium storage of the Li-Ti-O compound nanorods
    Xi, Kai
    Li, Ying
    Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering, 2010, 39 (11): : 2051 - 2054
  • [22] PREPARATION OF BINARY AND TERNARY OXIDES BY MOLTEN SALT METHOD AND ITS ELECTROCHEMICAL PROPERTIES
    Reddy, M. V.
    Theng, L. Pei
    Soh, Hulbert
    Beichen, Z.
    Jiahuan, F.
    Yu, C.
    Ling, A. Yen
    Andreea, L. Y.
    Ng, C. H. Justin
    Liang, T. J. L. Galen
    Ian, M. F.
    An, H. V. T.
    Ramanathan, K.
    Kevin, C. W. J.
    Daryl, T. Y. W.
    Hao, T. Yi
    Loh, K. P.
    Chowdari, B. V. R.
    SOLID STATE IONICS: IONICS FOR SUSTAINABLE WORLD, 2013, : 265 - 280
  • [23] Controlled electrochemical preparation of ruthenium-carbon composite powder in molten salt
    Chen, Yunfei
    Rong, Wan
    Jia, Zhihua
    Dang, Rui
    Jiang, Ting
    JOURNAL OF ALLOYS AND COMPOUNDS, 2025, 1022
  • [24] A study of preparation of titanium metal by the electrochemical reduction of titanium dioxide in molten salt
    Liu, Songli
    SECOND INTERNATIONAL CONFERENCE ON MINING ENGINEERING AND METALLURGICAL TECHNOLOGY (MEMT 2011), 2011, 2 : 1 - 6
  • [25] Preparation and Electrochemical Lithium Storage of the Li-Ti-O Compound Nanorods
    Xi Kai
    Li Ying
    RARE METAL MATERIALS AND ENGINEERING, 2010, 39 (11) : 2051 - 2054
  • [26] Preparation of activated carbon by molten salt electrochemical method and adsorption and recovery on chromium
    Ying, Huijuan
    Guo, Pengzi
    Shen, Jiawei
    Zhang, Xudong
    Wei, Yi
    INDUSTRIAL CROPS AND PRODUCTS, 2024, 222
  • [27] Electrocapillarity at the interface between a room-temperature molten salt and an aqueous solution
    Kasahara, T
    Shigematsu, F
    Tsujioka, N
    Yamamoto, M
    Kakiuchi, T
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2003, 225 : U698 - U698
  • [28] Influence of Surface Groups on Electrochemical Properties of Molten Salt Synthesized Ti3C2Tx in Mild Aqueous Electrolytes
    Guan, Bin
    Ma, Guoliang
    Lin, Zifeng
    BATTERIES & SUPERCAPS, 2024, 7 (09)
  • [29] A New Sight on the Influence of Molten Salt in the Preparation of (Ta, Nb, Ti) C Nanopowder
    Song, Weilong
    Chen, Zhaoke
    Chen, Shiyan
    Wu, Zongxu
    Xie, Fengminyu
    Wen, Qingbo
    Xiong, Xiang
    ADVANCED ENGINEERING MATERIALS, 2024, 26 (18)
  • [30] Solution heat treatment of Ti-Nb alloys using a molten salt shield
    Signor, Fernanda
    Pereira, Jonas Felipe
    Faita, Fabricio Luiz
    Bram, Martin
    Daudt, Natalia de Freitas
    MATERIALS LETTERS, 2023, 338
12345