Syntheses, Crystal Structures, and Spectra Properties of Two New M(II) [M = Cu and Ni] Macrocyclic Complexes

被引：0

作者：

Ren, Shi ^{[1
]}

Ma, Shu-Lin ^{[1
]}

机构：

[1] Tianjin Univ Commerce, Coll Sci, Dept Applicat Chem, Tianjin 300134, Peoples R China

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2012年 / 42卷 / 08期

关键词：

H-bond; macrocyclic complex; tetraaza macrocyclic; 3D network structure; MAGNETIC-PROPERTIES; COPPER(II) COMPLEXES; ZINC(II) COMPLEXES; NICKEL(II); ASSEMBLIES; COMPOUND; WATER; MODE;

D O I：

10.1080/15533174.2012.680143

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two new macrocyclic complexes, [ML](ClO4)(2)center dot 4,4'-bpy [M = Cu (1) and Ni (2), L = 1,3,6,9,11,14-hexaazatricyclo [12.2.1.1(6,9)]octadecane, 4,4'-bpy = 4,4'-bipyridine], have been synthesized and structurally characterized by X-ray crystallography analyses. Complex 1 crystallizes in the triclinic crystalline system of space group P-1, while complex 2 crystallizes in the monoclinic crystalline system of space group P2(1)/n. In the both complexes, M(II) [M = Cu (1) and Ni (2)] centers are located in a distorted square plane environment. The weakly interactions raised the structure unit to a 3D network.

引用

页码：1105 / 1109

页数：5

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