Self-assembly of halogen adducts of ester and carboxylic acid functionalised 1,3-dithiole-2-thiones

被引：9
|
作者：
Skabara, PJ
Berridge, R
Bricklebank, N
Lath, H
Coles, SJ
Horton, PN
机构：
[1] Univ Strathclyde, Dept Pure & Appl Chem, Glasgow G1 1XL, Lanark, Scotland
[2] Sheffield Hallam Univ, Ctr Biomed Res, Sheffield S1 1WB, S Yorkshire, England
[3] Univ Southampton, Dept Chem, Southampton SO17 1BJ, Hants, England
来源：
POLYHEDRON | 2006年 / 25卷 / 04期
关键词：
dihalogen adducts; supramolecular chemistry; X-ray crystallography;
D O I：
10.1016/j.poly.2005.11.013
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
New halogen adducts of 1,3-dithiole-2-thione-4-carboxylic acid and dimethyl 1,3-dithiole-2-thione-4,5-dicarboxylate have been prepared and characterised by X-ray crystallographic studies. The adducts feature an array of intramolecular and intermolecular close contacts involving chalcogen-chalcogen, chalcogen-halogen and halogen-halogen interactions. Whilst these contacts are derived from the basic heterocyclic unit and the coordinated halogen molecules, the ester and acid functionalities provide a varied and rich array of hydrogen bonding motifs, which significantly enhance the long-range order of the supramolecular structures. (c) 2005 Elsevier Ltd. All rights reserved.
引用
收藏
页码：989 / 995
页数：7
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