Crystal structure of N-(tert-Butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)cyclohexane carboxamide

被引：0
|
作者：
Habibi, Azizollah [1 ]
Yazdanbakhsh, Mohammad R. [2 ]
Mousavifar, Leyla [1 ,2 ]
机构：
[1] Tarbiat Moallem Univ, Fac Chem, Tehran, Iran
[2] Guilan Univ, Dept Chem, Guilan, Iran
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2008年 / 38卷 / 09期
关键词：
isoxazole; isocyanide; Alkylidene Meldrum's acid; X-ray analysis;
D O I：
10.1007/s10870-008-9379-x
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The crystal structure of N-(tert-butyl)-1-( 3, 5-dioxo-2-phenyltetrahydro-4-isoxazolyl)-cyclohexane-carboxamide 1 has been determined. The title compound crystallized in the orthorhombic space group pbca with cell parameters, a = 10.6556(6) angstrom, b = 18.0132(11) angstrom, c = 19.5513(12) angstrom, v = 3752.7( 4) angstrom(3), Z = 8, D-cal = 1.269 Mg/m(3) at T = 120 K. The structure refined by full-matrix least-squares procedures to find R-1 = 0.0463 and wR(2) = 0.0937 for 3059 reflections. The soxazole ring isn't coplanar with the phenyl ring.
引用
收藏
页码：701 / 704
页数：4
相关论文
共 50 条
  • [41] 2,6-DI-TERT-BUTYL-4-METHYLPHENYL ESTER OF N-[2,4,6-TRI(TERT-BUTYL)PHENYL]IMIDOPHOSPHENIC ACID
    ROMANENKO, VD
    RUBAN, AV
    DRAPAILO, AB
    POVOLOTSKII, MI
    MARKOVSKII, LN
    ZHURNAL OBSHCHEI KHIMII, 1987, 57 (01): : 235 - 236
  • [42] 1-tert-butyl-2-(tert-butoxysulfanyl)-1-(3,5-dimethylbenzoyl)2-(4-ethylbenzoyl)hydrazine
    Shang, Jian
    Wang, Qing-Min
    Huang, Run-Qiu
    Chen, Li
    Guo, Jian-Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O3778 - O3779
  • [43] 3-(tert-Butyl)-N-(4-methoxybenzyl)-1-methyl-1H-pyrazol-5-amine
    Becerra, Diana
    Rojas, Hugo
    Castillo, Juan-Carlos
    MOLBANK, 2021, 2021 (01)
  • [44] AN AXIAL TERT-BUTYL GROUP - CRYSTAL-STRUCTURE OF 1-PHENYL-C-4-TERT-BUTYL-R-CYCLOHEXYLPIPERIDINE HYDROCHLORIDE
    GENESTE, P
    KAMENKA, JM
    ROQUES, R
    DECLERCQ, JP
    GERMAIN, G
    TETRAHEDRON LETTERS, 1981, 22 (10) : 949 - 950
  • [45] 2,4-Di-tert-butyl-6-[1-(3,5-di-tert-butyl-2-hydroxyphenyl)ethyl]phenyl 4-methylbenzenesulfonate
    Wu, Jincai
    Pan, Xiaobo
    Wang, Lei
    Yao, Lihui
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O155 - U2615
  • [46] Crystal structure of (E)-2-[3-(tert-butyl)-2-hydroxy-benzylidene]-N-cyclohexylhydrazine-1-carbothioamide
    Arafath, Md Azharul
    Kwong, Huey Chong
    Adam, Farook
    Razali, Mohd R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 1460 - +
  • [47] Enantioselective Alkylation of N-(Diphenylmethylene) glycinate tert-Butyl Ester: Synthesis of (R)-2-(Benzhydrylidenamino)-3Phenylpropanoic Acid tert-Butyl Ester
    Shirakawa, Seiji
    Yamamoto, Kenichiro
    Liu, Kun
    Maruoka, Keiji
    ORGANIC SYNTHESES, 2013, 90 : 112 - +
  • [48] Synthesis, Crystal Structure and Biological Activity of N-(tert-butyl)-N′-(2-(4-chlorophenyl)acetyl)-5-methyl-1,2,3-thiadiazole-4-carbohydrazide
    Wang Dun
    Mao Wu-Tao
    Fan Zhi-Jin
    Li Juan-Juan
    Huang Yun
    Song Hai-Bin
    Fan Qian
    Kalinina, Tatiana A.
    Tatiana, Glukhareva
    Yur'evich, Morzherin Yury
    Pavlovna, Belskaya N.
    Alekseevich, Bakulev V.
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2013, 32 (05) : 673 - 678
  • [49] Synthesis, Crystal Structure and Antitumor Activity of 4-(tert-butyl)-5-(1H-1,2,4-triazol-1-yl)-N-(2-hydroxy-3,5-diiodinebenzyl)-thiazol-2-amine
    Ye Jiao
    Xie Xuan-Qing
    Li Kang-Ming
    Liu Yong-Chao
    Sun Li
    Hu Ai-Xi
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2015, 34 (03) : 344 - 348
  • [50] Synthesis, Crystal Structure and Antitumor Activity of 4-(tert-butyl)-5-(1H-1,2,4-triazol-1-yl)-N-(2-hydroxy-3,5-diiodinebenzyl)-thiazol-2-amine
    叶姣
    谢选青
    李康明
    刘永超
    孙利
    胡艾希
    结构化学, 2015, 34 (03) : 344 - 348
12345