Crystal structure of N-(tert-Butyl)-1-(3,5-dioxo-2-phenyltetrahydro-4-isoxazolyl)cyclohexane carboxamide

被引：0
|
作者：
Habibi, Azizollah [1 ]
Yazdanbakhsh, Mohammad R. [2 ]
Mousavifar, Leyla [1 ,2 ]
机构：
[1] Tarbiat Moallem Univ, Fac Chem, Tehran, Iran
[2] Guilan Univ, Dept Chem, Guilan, Iran
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2008年 / 38卷 / 09期
关键词：
isoxazole; isocyanide; Alkylidene Meldrum's acid; X-ray analysis;
D O I：
10.1007/s10870-008-9379-x
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The crystal structure of N-(tert-butyl)-1-( 3, 5-dioxo-2-phenyltetrahydro-4-isoxazolyl)-cyclohexane-carboxamide 1 has been determined. The title compound crystallized in the orthorhombic space group pbca with cell parameters, a = 10.6556(6) angstrom, b = 18.0132(11) angstrom, c = 19.5513(12) angstrom, v = 3752.7( 4) angstrom(3), Z = 8, D-cal = 1.269 Mg/m(3) at T = 120 K. The structure refined by full-matrix least-squares procedures to find R-1 = 0.0463 and wR(2) = 0.0937 for 3059 reflections. The soxazole ring isn't coplanar with the phenyl ring.
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收藏
页码：701 / 704
页数：4
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