Fatty ethylhydrazide from palm oil: chemical synthesis and characterization

被引：0
|
作者：
Jaloob, A. Guo [1 ]
Yeong, Tee Ta [1 ]
机构：
[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China
来源：
RESEARCH ON CHEMICAL INTERMEDIATES | 2013年 / 39卷 / 09期
关键词：
Fatty ethylhydrazide; Palm oil; Chemical synthesis; MODIFIED CLAY NANOCOMPOSITES; ENZYMATIC-SYNTHESIS; AMIDES; ACIDS;
D O I：
10.1007/s11164-012-0943-9
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this study, palm oil was reacted with ethylhydrazine in hexane by a refluxing method to produce fatty ethylhydrazides (FEHs). Glycerol was produced as a by-product. FEHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy, and H-1 nuclear magnetic resonance techniques. The results showed that a 6:1 molar ratio of palm oil to ethylhydrazine, giving about 76 % maximum conversion of palm oil into FEHs, and an 11-h reaction time are the optimum reaction conditions.
引用
收藏
页码：4269 / 4275
页数：7
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