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Effects of the main compositions in bath on the surface topography and electrocatalytic hydrogen evolution of Ni-Mo alloy films
被引:0
|作者:
Du J.
[1
]
Xie S.
[1
]
Li N.
[2
]
Xu L.
[1
]
机构:
[1] School of Packaging and Materials Engineering, Hunan University of Technology, Zhuzhou
[2] School of Metallurgical Engineering, Hunan University of Technology, Zhuzhou
来源:
基金:
中国国家自然科学基金;
关键词:
Cathode Polarization Curves;
Electrocatalytic Activities;
Hydrogen Evolution Reaction;
Ni-Mo Alloy Electrodes;
D O I:
10.1166/jamr.2016.1289
中图分类号:
学科分类号:
摘要:
The Ni-Mo alloy electrodes were prepared by electrodeposition technique with citric acid as a complexing agent. The influence of main compositions in bath such as the concentration of Na2MoO4 • 2H2O, the concentration of NiSO4 •6H2O and the concentration of sodium citrate on the microstructure and surface morphology of Ni-Mo alloy electrodes were characterized by scanning electron microscope (SEM). The hydrogen evolution reaction of Ni-Mo alloy electrodes were investigated in alkaline solution by the method of the cathode polarization curves. The results showed that the excellent Ni-Mo alloy electrodes with excellent electrocatalytic activities for hydrogen evolution were obtained when the concentration of Na2MoO4 •2H2O was 15 g/L, the concentration of NiSO4 •6H2O was 40 g/L, the concentration of sodium citrate concentration was 40 g/L. Copyright © 2016 American Scientific Publishers All rights reserved.
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页码:50 / 54
页数:4
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