Effects of the main compositions in bath on the surface topography and electrocatalytic hydrogen evolution of Ni-Mo alloy films

被引:0
|
作者
Du J. [1 ]
Xie S. [1 ]
Li N. [2 ]
Xu L. [1 ]
机构
[1] School of Packaging and Materials Engineering, Hunan University of Technology, Zhuzhou
[2] School of Metallurgical Engineering, Hunan University of Technology, Zhuzhou
来源
Xu, Lijian | 1600年 / American Scientific Publishers卷 / 11期
基金
中国国家自然科学基金;
关键词
Cathode Polarization Curves; Electrocatalytic Activities; Hydrogen Evolution Reaction; Ni-Mo Alloy Electrodes;
D O I
10.1166/jamr.2016.1289
中图分类号
学科分类号
摘要
The Ni-Mo alloy electrodes were prepared by electrodeposition technique with citric acid as a complexing agent. The influence of main compositions in bath such as the concentration of Na2MoO4 • 2H2O, the concentration of NiSO4 •6H2O and the concentration of sodium citrate on the microstructure and surface morphology of Ni-Mo alloy electrodes were characterized by scanning electron microscope (SEM). The hydrogen evolution reaction of Ni-Mo alloy electrodes were investigated in alkaline solution by the method of the cathode polarization curves. The results showed that the excellent Ni-Mo alloy electrodes with excellent electrocatalytic activities for hydrogen evolution were obtained when the concentration of Na2MoO4 •2H2O was 15 g/L, the concentration of NiSO4 •6H2O was 40 g/L, the concentration of sodium citrate concentration was 40 g/L. Copyright © 2016 American Scientific Publishers All rights reserved.
引用
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页码:50 / 54
页数:4
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