SOME EFFECTIVE SOLVENTS FOR RAPID AND RELIABLE CHARACTERIZATION OF PHENYLTHIOHYDANTOIN - AMINO-ACIDS .1. TLC WITH ABOUT 5 NANOMOLES OF SOLUTES

被引：5

作者：

MUNIER, RL ^{[1
]}

DRAPIER, AM ^{[1
]}

机构：

[1] INST PASTEUR, CNRS, 28 RUE DOCTEUR ROUX, F-75015 PARIS, FRANCE

来源：

CHROMATOGRAPHIA | 1979年 / 12卷 / 08期

关键词：

D O I：

10.1007/BF02265472

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

One-dimensional chromatography with internal standards permits reliable identification of the phenylthiohydantoins from all the common amino acids with the following TLC systems: silica gel-chloroform/n-butyl acetate (90:10), di-isopropylether/ethanol (95:5), dichloromethane/ethanol/acetic acid (90:8:2) or trans-dichloroethylene/ethanol/acetic acid (88:10:2); and cellulose with 25% formic acid-heptane/isobutanol/75% formic acid (40:30:9) or silica gel-chloroform/ethanol/acetic acid/water (50:47:0.5:2.5).

引用

页码：548 / 554

页数：7