SOME EFFECTIVE SOLVENTS FOR RAPID AND RELIABLE CHARACTERIZATION OF PHENYLTHIOHYDANTOIN - AMINO-ACIDS .1. TLC WITH ABOUT 5 NANOMOLES OF SOLUTES

被引：5

作者：

MUNIER, RL ^{[1
]}

DRAPIER, AM ^{[1
]}

机构：

[1] INST PASTEUR, CNRS, 28 RUE DOCTEUR ROUX, F-75015 PARIS, FRANCE

来源：

CHROMATOGRAPHIA | 1979年 / 12卷 / 08期

关键词：

D O I：

10.1007/BF02265472

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

One-dimensional chromatography with internal standards permits reliable identification of the phenylthiohydantoins from all the common amino acids with the following TLC systems: silica gel-chloroform/n-butyl acetate (90:10), di-isopropylether/ethanol (95:5), dichloromethane/ethanol/acetic acid (90:8:2) or trans-dichloroethylene/ethanol/acetic acid (88:10:2); and cellulose with 25% formic acid-heptane/isobutanol/75% formic acid (40:30:9) or silica gel-chloroform/ethanol/acetic acid/water (50:47:0.5:2.5).

引用

页码：548 / 554

页数：7

共 41 条

[31] STUDY OF TRANS-ANNULAR INTERACTION OF SOME AMINO-ACIDS AND GLYCYLGLYCINE WITH 1,2,5,6-DIBENZO-3,3,7,7-TETRAMETHYLCYCLOOCTANDION-4,8
LAGIDZE, LM
IREMADZE, NK
CHIGOGIDZE, LP
LAGIDZE, DR
DEVDARIANY, RR
ROZINOV, BV
KHIMIYA PRIRODNYKH SOEDINENII, 1979, (01): : 43 - 48
[32] VOLUMETRIC AND SOLVATION BEHAVIOR OF AMINO-ACIDS IN SOME AQUEOUS BINARIES .1. GLYCINE, DL-ALANINE, AND DL-ALPHA-AMINOBUTYRIC ACID IN AQUEOUS-SOLUTIONS OF STRONG ELECTROLYTES
BASUMALLICK, IN
MOHANTY, RK
CHAKRABORTY, U
INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 1986, 25 (12): : 1089 - 1091
[33] METAL-COMPLEXES OF AMINO-ACIDS AND DERIVATIVES .13. SOME NICKEL(II) COMPLEXES OF L-ARGININE ZWITTERIONS OR L-ARGININATE ANIONS - NOVEL IONIC -] BIDENTATE PERCHLORATE REARRANGEMENT BROUGHT ABOUT BY PRESSURE[1-5]
CHOW, ST
MCAULIFFE, CA
JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1975, 37 (04): : 1059 - 1064
[34] PHARMACOKINETIC CHARACTERIZATION OF THE POSTDISTRIBUTION PHASE OF PROHORMONE ATRIAL NATRIURETIC PEPTIDES AMINO-ACIDS 1-98, 31-67, AND ATRIAL-NATRIURETIC-FACTOR DURING AND AFTER RAPID RIGHT VENTRICULAR PACING IN DOGS
ACKERMAN, BH
WYETH, RP
VESELY, DL
NGO, WL
BISSETT, JK
WINTERS, CJ
SALLMAN, AL
JOURNAL OF CLINICAL PHARMACOLOGY, 1992, 32 (05): : 415 - 421
[35] H-1, C-13 AND N-15 RANDOM COIL NMR CHEMICAL-SHIFTS OF THE COMMON AMINO-ACIDS .1. INVESTIGATIONS OF NEAREST-NEIGHBOR EFFECTS (VOL 5, PG 67, 1995)
WISHART, DS
BIGAM, CG
HOLM, A
HODGES, RS
SYKES, BD
JOURNAL OF BIOMOLECULAR NMR, 1995, 5 (03) : 332 - 332
[36] MIXED COMPLEXES OF AMINO-ACIDS WITH TRANSITION-METALS .1. PREPARATION AND CHARACTERIZATION OF THE NEW MIXED COMPLEX CU-II(L-TRYPTOPHANATE)(DL-METHIONINATE).1.5H2O
GILI, P
ZARZA, PM
INORGANICA CHIMICA ACTA-ARTICLES AND LETTERS, 1984, 89 (02): : L23 - L25
[37] ANGIOTENSIN-II ANALOGS .1. SYNTHESIS AND INCORPORATION OF THE ALOGENATED AMINO-ACIDS 3-(4'-IODOPHENYL)ALANINE, 3-(3',5'-DIBROMO-4'-CHLOROPHENYL)ALANINE,3-(3',4',5'-TRIBROMOPHENYL)ALANINE, AND 3-(2',3',4',5',6'-PENTABROMOPHENYL)ALANINE
LEDUC, R
BERNIER, M
ESCHER, E
HELVETICA CHIMICA ACTA, 1983, 66 (03) : 960 - 970
[38] SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF MIXED-FLUORO COMPLEXES OF UO22+ CONTAINING AMINO-ACIDS, ACETYLACETONATE OR ACETATE AS THE CO-LIGANDS AND THE 1ST REPORT ON THE HEPTAFLUORODIOXOURANATE(VI) COMPLEX [UO2F7]5-
CHAUDHURI, MK
SRINIVAS, P
KHATHING, DT
POLYHEDRON, 1993, 12 (02) : 227 - 234
[39] STRUCTURE AND CONFORMATION OF SPIN-LABELED AMINO-ACIDS IN FROZEN-SOLUTIONS DETERMINED BY ELECTRON NUCLEAR DOUBLE-RESONANCE .1. METHYL N-(2,2,5,5-TETRAMETHYL-1-OXYPYRROLINYL-3-CARBONYL)-L-ALANATE, A MOLECULE WITH A SINGLE PREFERRED CONFORMATION
MUSTAFI, D
SACHLEBEN, JR
WELLS, GB
MAKINEN, MW
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1990, 112 (07) : 2558 - 2566
[40] SYNTHESIS, OPTICAL RESOLUTION AND RADIOLYSIS OF TERTIARY AMINO-ACIDS WITH HIGHLY SPECIFIC ACTIVITIES .1. D,L-LYSINE(H-3-4,5,6,6) - L-LYSINE (H-3-4,4,5,5) - L-LEUCINE(H-3-4,5,5,5) - D-ALPHA-AMINO ADIPIC ACID (3H-4,4,5,5) - GAMMA-AMINOBUTYRIC-ACID (H-3-2,2,3,3)
EGO, D
BEAUCOURT, JP
PICHAT, L
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 1986, 23 (03): : 229 - 244

← 1 2 3 4 5 →