SOME EFFECTIVE SOLVENTS FOR RAPID AND RELIABLE CHARACTERIZATION OF PHENYLTHIOHYDANTOIN - AMINO-ACIDS .1. TLC WITH ABOUT 5 NANOMOLES OF SOLUTES

被引：5

作者：

MUNIER, RL ^{[1
]}

DRAPIER, AM ^{[1
]}

机构：

[1] INST PASTEUR, CNRS, 28 RUE DOCTEUR ROUX, F-75015 PARIS, FRANCE

来源：

CHROMATOGRAPHIA | 1979年 / 12卷 / 08期

关键词：

D O I：

10.1007/BF02265472

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

One-dimensional chromatography with internal standards permits reliable identification of the phenylthiohydantoins from all the common amino acids with the following TLC systems: silica gel-chloroform/n-butyl acetate (90:10), di-isopropylether/ethanol (95:5), dichloromethane/ethanol/acetic acid (90:8:2) or trans-dichloroethylene/ethanol/acetic acid (88:10:2); and cellulose with 25% formic acid-heptane/isobutanol/75% formic acid (40:30:9) or silica gel-chloroform/ethanol/acetic acid/water (50:47:0.5:2.5).

引用

页码：548 / 554

页数：7

共 41 条

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LEYENDEKKERS, JV
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[2] ADSORPTION BEHAVIOR OF SOME AMINO-ACIDS ON CHEMICALLY PRETREATED ALUMINA .1.
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JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1984, 97 (02) : 582 - 584
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SOUTH AFRICAN JOURNAL OF CHEMISTRY, 1978, 31 (03) : 77 - 80
[4] MOLECULAR POLARIZABILITIES OF SOME AMINO-ACIDS .1. GLYCINE AND L-ALANINE
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GUPTA, VD
MEHROTRA, C
PRAMANA, 1981, 16 (05) : 369 - 373
[5] STUDIES OF UNUSUAL AMINO-ACIDS AND THEIR PEPTIDES .12. THE CHEMISTRY OF N-(CARBOXYMETHYL) AMINO-ACIDS .1. THE PREPARATION, PROPERTIES, AND CHARACTERIZATION OF N-(CARBOXYMETHYL) AMINO-ACIDS AND THEIR ESTERS
MIYAZAWA, T
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1980, 53 (09) : 2555 - 2565
[6] STUDIES IN SOME PHYSICAL-PROPERTIES OF AMINO-ACIDS .1. SPECIFIC ROTATIONS, APPARENT MOLAL VOLUMES AND ADIABATIC COMPRESSIBILITIES OF L-AMINO-ACIDS IN MIXED-SOLVENTS
JAHAGIRDAR, DV
PANKANTI, SU
INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 1983, 22 (03): : 195 - 197
[7] INVESTIGATIONS ON ANALYSIS OF AMINO-ACIDS IN SURFACE WATER .1. BEHAVIOR OF SOME ACID AND NEUTRAL AMINO-ACIDS DURING PRECONCENTRATION AND DESALTING BY ION-EXCHANGE
KRUTZ, M
FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1975, 273 (02): : 123 - 126
[8] STUDIES ON MIXED-LIGAND COMPLEXES OF CADMIUM ION WITH SOME AMINO-ACIDS AND MALONIC-ACIDS .1.
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CHEMICA SCRIPTA, 1982, 20 (05): : 229 - 233
[9] THE INFLUENCE OF VARIOUS FACTORS ON THE OPTICAL-ACTIVITY OF SOME ESSENTIAL AMINO-ACIDS .1. APPLICATIONS
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STASESCU, LA
REVUE ROUMAINE DE CHIMIE, 1987, 32 (11-12) : 1045 - 1050
[10] STUDY ON CARBOXYL-ACTIVATION OF AMINO-ACIDS USING A 4-NITROSO-5-AMINO-PYRAZOLE .1.
GUARNERI, M
GIORI, P
FERRONI, R
TOMATIS, R
BENASSI, CA
GAZZETTA CHIMICA ITALIANA, 1973, 103 (10-1): : 1105 - 1111

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