N-(4-Chloro-3-nitrophenyl)maleamic acid

被引：1

作者：

Chaithanya, U. ^{[1
]}

Foro, Sabine ^{[2
]}

Gowda, B. Thimme ^{[1
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalagangothri 574199, Karnataka, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 13.3; mean σ(C-C) = 0.006 Å; R factor = 0.063; single-crystal X-ray study; T = 293 K; wR factor = 0.180;

D O I：

10.1107/S1600536812008021

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the mol-ecule of the title compound,C 10H 7ClN 2O 5, the acyclic C=C double bond is cis configured. The C=O and O - H bonds of the acid group are in a relatively rare anti position to each other, due to the donation of intramolecular hydrogen bond to the amide by the carboxyl group. The nitro group is significantly twisted [dihedral angle = 66.9 (3)°] out of the plane of the remaining atoms, which are almost coplanar (r.m.s. deviation for non-H atoms except the nitro group = 0.202 Å). In the crystal, N - H⋯O hydrogen bonds link the mol-ecules into zigzag chains running along the b axis.

引用

页码：O873 / U3202

页数：7

共 50 条

[41] N-(2,5-Dichlorophenyl)maleamic acid
Shakuntala, K.
Gowda, B. Thimme
Tokarcik, Miroslav
Kozisek, Jozef
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O3119 - U839
[42] N-(4-chloro-2-nitrophenyl)-N-methyl-N′-(quinolin-4-ylmethylene) hydrazine
Karadayi, N
Aydemir, E
Kazak, C
Kirpi, E
Tugcu, FT
Gümüs, MK
Kaban, S
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2671 - O2673
[43] ALPHA-[4-CHLORO-3-NITROPHENYL]-BETA-AMINOETHANOLS - POTENTIAL BETA-ADRENERGIC BLOCKING-AGENTS
SHAFIK, RM
SOLIMAN, FSG
PHARMAZIE, 1976, 31 (07): : 481 - 482
[44] Synthesis, crystal structure,anti-tuberculosis activity and toxicity prediction of N-(4-bromophenyl)-3-(5-(4-chloro-3-nitrophenyl)-1,3,4-oxadiazol-2-yl) benzenesulfonamide
Fan, Chao
Chen, Jianchao
Xu, Zhongkai
Yin, Peng
Wu, Chengjun
Sun, Tiemin
JOURNAL OF MOLECULAR STRUCTURE, 2024, 1297
[45] N-(4-Methyl-2-nitrophenyl)succinamic acid
Chaithanya, U.
Foro, Sabine
Gowda, B. Thimme
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O819 - U2824
[46] Synthesis, spectroscopic studies and biological applications of organotin(IV) derivatives of 3-[N-(4-nitrophenyl)-amido]propenoic acid and 3-[N-(4-Nitrophenyl)-amido]propanoic acid
Department of Chemistry, Quaid-i-Azam University, Islamabad 45320, Pakistan
Bull. Korean Chem. Soc., 2006, 1 (44-52):
[47] Phenyl N-(5-chloro-2-nitrophenyl)-carbamate
Zou, Bao-Hua
Fang, Zheng
Zhong, Hui
Kai, Guo
Wei, Ping
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02547 - +
[48] N-(4-nitrophenyl)-N′-phenylsuccinamide
Butcher, Ray J.
Jasinski, Jerry P.
Ravindra, H. J.
Dharmaprakash, S. M.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4367 - U3879
[49] N-(3-Chloro-4-fluorophenyl)acetamide
Fun, Hoong-Kun
Loh, Wan-Sin
Shetty, Divya N.
Narayana, B.
Sarojini, B. K.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1348 - +
[50] N-(3-chloro-4-fluorophenyl)thiourea
Rosli, Mohd Mustaqim
Karthikeyan, Mari Sithambaram
Fun, Hoong-Kun
Razak, Ibrahim Abdul
Patil, P. S.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O67 - O68

← 1 2 3 4 5 →