N-(4-Chloro-3-nitrophenyl)maleamic acid

被引：1

作者：

Chaithanya, U. ^{[1
]}

Foro, Sabine ^{[2
]}

Gowda, B. Thimme ^{[1
]}

机构：

[1] Mangalore Univ, Dept Chem, Mangalagangothri 574199, Karnataka, India

[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

data-to-parameter ratio = 13.3; mean σ(C-C) = 0.006 Å; R factor = 0.063; single-crystal X-ray study; T = 293 K; wR factor = 0.180;

D O I：

10.1107/S1600536812008021

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the mol-ecule of the title compound,C 10H 7ClN 2O 5, the acyclic C=C double bond is cis configured. The C=O and O - H bonds of the acid group are in a relatively rare anti position to each other, due to the donation of intramolecular hydrogen bond to the amide by the carboxyl group. The nitro group is significantly twisted [dihedral angle = 66.9 (3)°] out of the plane of the remaining atoms, which are almost coplanar (r.m.s. deviation for non-H atoms except the nitro group = 0.202 Å). In the crystal, N - H⋯O hydrogen bonds link the mol-ecules into zigzag chains running along the b axis.

引用

页码：O873 / U3202

页数：7

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