POLYMER-SUPPORTED SOLUTION SYNTHESIS OF A HEPTAGLUCOSIDE HAVING PHYTOALEXIN ELICITOR ACTIVITY

被引：0
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作者：
VERDUYN, R
VANDERKLEIN, PAM
DOUWES, M
VANDERMAREL, GA
VANBOOM, JH
机构：
来源：
RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS-JOURNAL OF THE ROYAL NETHERLANDS CHEMICAL SOCIETY | 1993年 / 112卷 / 7-8期
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中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient synthesis of methyl heptaglucoside 2 using poly(ethyleneglycol)monomethyl ether as a polymer support is described. Elongation of the acceptor 11, anchored via a succinoyl linkage to PEG, with the appropriate glycosyl donors 4-6 and intermittent protective group manipulations gave fully protected heptamer 18. Deprotection of 18 furnished, after purification as its peracetate, title compound 2 in a good overall yield.
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页码：464 / 466
页数：3
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