EVALUATION OF A SPLIT-TYPE FLOW CELL FOR A POLARIZED SPECTROPHOTOMETRIC DETECTOR

被引:14
|
作者
YAMAMOTO, A
MATSUNAGA, A
MIZUKAMI, E
HAYAKAWA, K
MIYAZAKI, M
NISHIMURA, M
KITAOKA, M
FUJITA, T
机构
[1] KANAZAWA UNIV,FAC PHARMACEUT SCI,KANAZAWA,ISHIKAWA 920,JAPAN
[2] SHIMADZU CO LTD,NAKAGYO KU,KYOTO 604,JAPAN
关键词
POLARIZED SPECTROPHOTOMETRIC DETECTOR; SPLIT-TYPE FLOW CELL; HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY;
D O I
10.1039/an9952001137
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A split-type flow cell for a polarized spectrophotometric detector (PPD), in which the column effluent is simultaneously passed through both the sample and reference sides, is described. The improvement in detection sensitivity in PPD with the use of this cell is discussed. Its utility as a universal polarimetric detector for HPLC for the detection of coloured amino acid-copper(II) complexes is shown. A new possibility for this cell in the gradient elution separation of glucose syrup is demonstrated.
引用
收藏
页码:1137 / 1139
页数:3
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