SYNTHESIS OF SOME NEW HETEROCYCLIC-COMPOUNDS CONTAINING THIENO[2,3-B]QUINOLINE MOIETY

被引：12

作者：

ABDELRAHMAN, AE ^{[1
]}

AWAD, IMA ^{[1
]}

BAKHITE, EA ^{[1
]}

机构：

[1] UNIV ASSIUT,FAC SCI,DEPT CHEM,ASSIUT,EGYPT

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1991年 / 60卷 / 3-4期

关键词：

THIENOQUINOLINES; PYRIMIDINE-DITHIONES; PYRIMIDINE-DITHIOETHERS; CHLOROTRIAZINES; MERCAPTOTRIAZINES; HYDRAZINOTRIAZINES AND PYRAZOLYLTRIAZINES;

D O I：

10.1080/10426509108036781

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

2-Cyano-3-amino-4-aryl-5, 6, 7, 8-tetrahydro-thieno[2, 3-b]quinoline (1) reacted with carbon disulfide to give compound 2. Alkylation of 2 with different reagents gave the corresponding thioethers 3-7. Diazotisation of 1 furnished chloro derivative 8 which reacted with thiourea to give mercaptotriazine 9. Methylation of 9 yielded 10. On treatment of 8 with hydrazone hydrate, the expected hydrazinocompound 11 was obtained. Reaction of 11 with aromatic aldehydes, acetylacetone, acetic acid, acetic anhydride, carbon disulfide and nitrous acid gave compounds 12-17, respectively. The structures of all synthesized compounds were confirmed by elemental and spectral analysis. © 1991, Taylor & Francis Group, LLC. All rights reserved.

引用

页码：189 / 199

页数：11

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