A FACILE SYNTHESIS OF THE INTERMEDIATES OF THE BICYCLIC ORGANIC-BASES - DBU AND TBD

被引：5
|
作者：
CHENG, XH [1 ]
LIU, FC [1 ]
机构：
[1] YUNNAN UNIV,DEPT CHEM,KUNMING 650091,PEOPLES R CHINA
来源：
SYNTHETIC COMMUNICATIONS | 1993年 / 23卷 / 22期
关键词：
D O I：
10.1080/00397919308011178
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Intermediates of DBU and TBD, N-(3-aminoproply) - epsilon-caprolactam and bis-(3-aminopropyl)-amine were prepared by the hydrogenolysis of N-(2-cyanoethyl) - epsilon - caprolactam and di- (beta-cyanoethyl)amine respectively over Raney-Ni in the presence of NaBH4 under atmospheric pressure with mild condition and good yield.
引用
收藏
页码：3191 / 3194
页数：4
相关论文
共 50 条
  • [31] PHARMACOKINETIC STUDIES OF THE PANCREATIC EXCRETION OF ORGANIC-BASES IN THE RAT
    MAICKEL, RP
    MCFADDEN, DP
    JOURNAL OF PHARMACOLOGICAL METHODS, 1979, 2 (04): : 323 - 332
  • [32] CHARACTERIZATION OF ORGANIC-BASES IN HYDROCRACKED SHALE OIL FUELS
    HARDY, D
    HAZLETT, RN
    SOLASH, J
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1982, 183 (MAR): : 52 - FUEL
  • [33] PROTONATION OF ORGANIC-BASES IN CLAY-WATER SYSTEMS
    KARICKHOFF, SW
    BAILEY, GW
    CLAYS AND CLAY MINERALS, 1976, 24 (04) : 170 - +
  • [34] EFFECT OF ORGANIC-BASES ON THE EXTRACTION OF GADOLINIUM CARBOXYLATE EXTRACTION
    SUKHAN, VV
    FRANKOVSKY, VA
    UKRAINSKII KHIMICHESKII ZHURNAL, 1982, 48 (01): : 59 - 60
  • [35] ARGENTOMETRIC DETERMINATION OF EPOXIDE COMPOUNDS IN PRESENCE OF ORGANIC-BASES
    DUOBINIS, NK
    KOLODZEISKIS, VS
    ZHEMAITAITIS, AI
    DAUETAS, AA
    JOURNAL OF ANALYTICAL CHEMISTRY OF THE USSR, 1976, 31 (05): : 841 - 843
  • [36] URANIUM EXTRACTION BY CAPROIC ACID IN THE PRESENCE OF ORGANIC-BASES
    SUKHAN, VV
    GORLACH, VF
    YAKIMENKO, LN
    UKRAINSKII KHIMICHESKII ZHURNAL, 1984, 50 (03): : 270 - 272
  • [37] Photocatalysis with organic dyes: facile access to reactive intermediates for synthesis
    Amos, Stephanie G. E.
    Garreau, Marion
    Buzzetti, Luca
    Waser, Jerome
    BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, 2020, 16 : 1163 - 1187
  • [38] THERMOCHEMISTRY OF TERTIARY BUTYL HYDROPEROXIDE SOLUTIONS IN ORGANIC-BASES
    SOLOVEVA, EI
    TSVETKOV, VG
    SULDIN, BV
    ALEKSANDROV, YA
    ZHURNAL OBSHCHEI KHIMII, 1979, 49 (07): : 1646 - 1649
  • [39] SPECTROSCOPIC DETERMINATION OF ASSOCIATION CONSTANTS OF WATER WITH ORGANIC-BASES
    LENARVOR, A
    GENTRIC, E
    LAURANSAN, J
    SAUMAGNE, P
    JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS I, 1976, 72 : 1329 - 1332
  • [40] STUDIES ON COMPLEXES OF PENTACYANOAMMINEFERRATE (II) AND SOME ORGANIC-BASES
    MALIK, WU
    BEMBI, R
    SINGH, YP
    CURRENT SCIENCE, 1976, 45 (15): : 540 - 541
12345