STRUCTURE OF BIS(4-BENZOYL-2,4-DIHYDRO-5-METHYL-2-PHENYL-3H-PYRAZOL-3-ONATO-O,O')DINITRATOBIS(TRIPHENYLPHOSPHINE OXIDE-O)THORIUM(IV)

被引：9
|
作者：
JARVINEN, GD
ZOZULIN, AJ
LARSON, EM
RYAN, RR
机构：
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1991年 / 47卷
关键词：
D O I：
10.1107/S0108270190002177
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
[Th(C17H13N2O2)2(NO3)2(C18H15OP)2], M(r) = 1467, orthorhombic, Pcan, a = 11.619 (10), b = 23.721 (10), c = 25.243 (4) angstrom, V = 6957.33 angstrom 3, Z = 4 D(x) = 1.40 g cm-3, lambda-(Mo K-alpha) = 0.71069 angstrom, mu = 23.2 cm-1, F(000) = 2936, T = 298 K, R = 0.058 for 2547 reflections with I greater-than-or-equal-to 2-sigma-(I). The crystal is composed of discrete molecules containing a thorium ion coordinated to ten O atoms from two bidentate benzoyl pyrazolone anions, two bidentate nitrate anions, and two triphenylphosphine oxide molecules.
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页码：262 / 264
页数：3
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