STRUCTURE OF METHYL 2-(2,5-DIHYDRO-2-OXO-3-PHENYL-5-FURYL)LACTATE

被引：0
|
作者：
HYNES, RC
机构：
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1992年 / 48卷
关键词：
D O I：
10.1107/S0108270191008399
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
C14H14O5, M(r) = 262.26, monoclinic, P2(1)/n, a = 11.319 (3), b = 6.5115 (15), c = 18.105 (5) angstrom, beta = 105.660 (20)-degrees, V = 1284.8 (6) angstrom 3, Z = 4, D(x) = 1.356 g cm-3, lambda(Cu K-alpha(1)) = 1.54056 angstrom, mu = 8.26 cm-1, F(000) = 553.89, T = 295 K, R = 0.036, wR = 0.033 for 1692 reflections with I > 2.5-sigma(I). The structure determination established the identity of the product of a Co2(CO)8-catalyzed carbonylation reaction with an epoxy alcohol.
引用
收藏
页码：395 / 396
页数：2
相关论文
共 50 条
  • [31] Ethyl (Z)-2-(2-fluorobenzylidene)-7-methyl-3-oxo-5-phenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate
    Zhao, Cheng-Guang
    Hu, Jie
    Zhang, Ya-Li
    Zhang, Jing
    Yang, Shu-Lin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3009 - U1167
  • [32] Synthesis of methyl 2-[(1,2-dihydro-4-hydroxy-2-oxo-1-phenylquinolin-3-yl) carbonylamino] alkanoates and methyl 2-[2-(4,2-dihydro-4-hydroxy-2-oxo-1-phenylquinolin-3-ypcarbonyl-amino)alkanamido] alkanoate
    Fathalla, Walid
    Pazdera, Pavel
    ARKIVOC, 2017, : 158 - 173
  • [33] 2-[(2-chloro-5-phenyl-3-pyridinyl)(hydroxy)methyl]acrylonitrile
    Swamy, GYSK
    Ravikumar, K
    Narender, P
    Rao, VJ
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O706 - O707
  • [34] METHYL 5-CYANO-1-[2-(METHYOXYCARBONYL)PHENYL]-4,5-DIHYDRO-3-PYRAZOLECARBOXYLATE
    PILATI, T
    CASALONE, G
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1994, 50 : 1503 - 1505
  • [35] Structure and proton-acceptor ability of 2-phenyl-, 2-(2-furyl)-, 2-(2-thienyl)-5-phenyloxazoles and their carbonyl derivatives
    Patsenker, LD
    Surov, YN
    Lokshin, AI
    Shkumat, AP
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 1999, 69 (11) : 1810 - 1816
  • [36] N-{4-Bromo-2-[(S)-menthyloxy]-5-oxo-2,5-dihydro-3-furyl}-L-valine
    Song, Xiu-Mei
    Li, Zhao-Yang
    Wang, Zhao-Yang
    Fu, Jian-Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1838 - U2804
  • [37] Synthesis of 2-(5-aryl-4-methyl-2-oxo-1,2-dihydro- 3H-pyrrol-3-ylidene)malononitriles
    M. Yu. Belikov
    M. Yu. Ievlev
    A. G. Milovidova
    O. V. Ershov
    Russian Journal of Organic Chemistry, 2017, 53 : 1601 - 1603
  • [38] MOLECULAR AND CRYSTAL-STRUCTURE OF THE 2 HYDRAZONE PIGMENTS N-(2-METHYLPHENYL)-2-(2-METHYL-PHENYL-HYDRAZONO)-3-OXO-BUTYRAMIDE AND N-(2-METHOXY-PHENYL)-2-(2-METHOXY-PHENYLHYDRAZONO)-3-OXO-BUTYRAMIDE
    PAULUS, EF
    RIEPER, W
    WAGNER, D
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1983, 165 (1-4): : 137 - 149
  • [39] Crystal structure of methyl (2Z)-2-[(2Z)-2-(2-cyclopentylidenehydrazin-1-yl-idene)-4-oxo-3-phenyl-1,3-thiazolidin-5-ylidene]ethanoate
    Akkurt, Mehmet
    Smolenski, Victoria A.
    Mohamed, Shaaban K.
    Jasinski, Jerry P.
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O776 - U515
  • [40] (Z)-Ethyl 2-(2,4-dimethylbenzylidene)-7-methyl-3-oxo-5-phenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate
    Chen, Xiao-Yan
    Wang, Han-Chu
    Zhang, Qian
    Song, Zhi-Jian
    Zheng, Fei-Yun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
12345