3,5-Bis[(pyridin-4-yl)methoxy]benzoic acid

被引：1
|
作者：
Lin, Hong [1 ]
Zhang, Yi-Ping [2 ]
机构：
[1] Jinhua Profess Tech Coll, 1188 Wuzhou St, Jinhua 321017, Zhejiang, Peoples R China
[2] Zhejiang Normal Univ, Inst Phys Chem, Zhejiang Key Lab React Chem Solid Surfaces, Jinhua 321004, Zhejiang, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词：
D O I：
10.1107/S1600536812049550
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Single crystals of the title compound, C19H16N2O4, were obtained under hydrothermal conditions by an unintended recrystallization of the employed microcrystalline starting material. The [(pyridin-4-yl) methoxy] benzoic acid unit is nearly planar, with a maximum deviation from the leastsquares plane of 0.194 (2) angstrom. This plane is inclined by 35.82 (6)degrees to that defined by the second (pyridin-4-yl) methoxy group [in which the largest deviation from the least-squares plane is 0.013 (2) angstrom]. In the crystal, molecules are linked by O-H center dot center dot center dot N hydrogen bonds involving the acid hydroxy group and a pyridine N atom into chains parallel to [201].
引用
收藏
页码：O77 / +
页数：8
相关论文
共 50 条
  • [41] REGIOSPECIFIC SYNTHESIS OF 3,5-BIS(BROMOMETHYL)BENZOIC ACID, A CYSTEINE CROSS-LINKING AGENT
    ENGEL, M
    BURRIS, CW
    SLATE, CA
    ERICKSON, BW
    TETRAHEDRON, 1993, 49 (39) : 8761 - 8770
  • [42] Synthesis of 3,5-Bis(hydroxymethyl)adamantan-1-ols and 3,5-Bis(nitrooxymethyl)adamantan-1-yl Nitrates
    Ivleva, E. A.
    Kazakova, A. I.
    Klimochkin, Yu. N.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2020, 56 (09) : 1562 - 1569
  • [43] Synthesis of 3,5-Bis(hydroxymethyl)adamantan-1-ols and 3,5-Bis(nitrooxymethyl)adamantan-1-yl Nitrates
    E. A. Ivleva
    A. I. Kazakova
    Yu. N. Klimochkin
    Russian Journal of Organic Chemistry, 2020, 56 : 1562 - 1569
  • [44] Three Coordination Polymers based on 3,5-Bis( imidazole-1-yl) pyridine and Benzoic Acid: Synthesis, Crystal Structures and Photoluminescent Properties
    Xu, Jiakun
    Yan, Xingchen
    Sun, Xiaochun
    Sun, Guolong
    Bi, Caifeng
    Sun, Mi
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2014, 640 (02): : 398 - 404
  • [45] Synthesis, characterization, and crystal structures of two coordination polymers from 3,5-bis(pyridin-4-ylmethyl) aminobenzoic acid
    Kuai, Hai-Wei
    Cheng, Xiao-Chun
    Zhu, Xiao-Hong
    JOURNAL OF COORDINATION CHEMISTRY, 2011, 64 (19) : 3323 - 3332
  • [46] Poly[bis{mu-N '-[(pyridin-4-yl)methylidene]benzohydrazidato}copper(II)]
    Wu, Qiong
    Chen, Da-Chi
    Wu, Chu-Yi
    Yan, Chang-Xiu
    Liao, Jian-Zhen
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M383 - +
  • [47] Synthesis of 3,5-bis(phosphonomethyl)benzoic acid and its application as a metal oxide surface bivalent anchor
    Nakhle, BM
    Trammell, SA
    Sigel, KM
    Meyer, TJ
    Erickson, BW
    TETRAHEDRON, 1999, 55 (10) : 2835 - 2846
  • [48] Study on structure and properties of two metal coordination polymers prepared by 3,5-Bis (4-carboxy-phenoxy)benzoic acid
    Liu, Xin
    Zhao, Lun
    Zhao, Changjiang
    Meng, Lingshu
    Liu, Chang
    JOURNAL OF MOLECULAR STRUCTURE, 2019, 1188 : 238 - 243
  • [49] 3,5-Bis(4-fluorophenyl)isoxazole
    Fun, Hoong-Kun
    Arshad, Suhana
    Samshuddin, S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1783 - +
  • [50] Synthesis of (2-Aminopyrimidin-4-yl)(pyridin-4-yl)methanone and Derivatives
    Giraud, Francis
    Josselin, Beatrice
    Ruchaud, Sandrine
    Anizon, Fabrice
    Moreau, Pascale
    SYNTHESIS-STUTTGART, 2023, 55 (22): : 3825 - 3832
12345