HIGHLY TWISTED SUBSTITUTED ARENES - X-RAY STRUCTURE AND DYNAMIC H-1-NMR SPECTRA OF 1,4-DIALKYL-2,3,5,6-TETRAKIS(ALKYLSULFONYL)BENZENES

被引：6

作者：

COLLARD, DM ^{[1
]}

SADRI, MJ ^{[1
]}

VANDERVEER, D ^{[1
]}

HAGEN, KS ^{[1
]}

机构：

[1] EMORY UNIV,DEPT CHEM,ATLANTA,GA 30322

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1995年 / 13期

关键词：

D O I：

10.1039/c39950001357

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The sulfonyl groups around 1,4-disubstituted-2,3,5,6-tetrakis(alkylsulfonyl)benzenes adopt an altering orientation and the ring is highly twisted, with external torsion angles (S-C-ar-C-ar-S) of 46 degrees and internal torsion angles(C-ar-C-ar-CarCar) of 23 degrees.

引用

页码：1357 / 1358

页数：2

共 50 条

[31] Haptotropic shifts in (C5H5)Fe and Mn(CO)(3) complexes of 4H-cyclopenta[def]phenanthrene (cppH): X-ray crystal structure and NMR fluxionality of (eta(1)-cpp)Mn(CO)(3)(PEt(3))(2)
Decken, A
Rigby, SS
Girard, L
Bain, AD
McGlinchey, MJ
ORGANOMETALLICS, 1997, 16 (06) : 1308 - 1315
[32] Selective complexation of uranium(III) over cerium(III) by 2,6-bis(5,6-dialkyl-1,2,4-triazin-3-yl)pyridines:: 1H NMR and X-ray crystallography studies
Iveson, PB
Rivière, C
Guillaneux, D
Nierlich, M
Thuéry, P
Ephritikhine, M
Madic, C
CHEMICAL COMMUNICATIONS, 2001, (16) : 1512 - 1513
[33] REACTION OF 1,4-DIENES WITH METAL-COMPLEXES .2. SYNTHESIS AND X-RAY STRUCTURE DETERMINATION OF (ETA-3-1-METHYLENE-3-METHYLCYCLOHEXYL)(TRIPHENYLPHOSPHINE)PALLADIUM(II), (C8H13)PDCLP(C6H5)3
ZEINER, H
RATKA, R
ZIEGLER, ML
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1977, 32 (02): : 172 - 177
[34] Molecular and crystalline structure of cycloheptanespiro-3′(4′H)-6′,7′,8′,9′-tetrahydrocyclohexa[b][1,4]thiazole-2′(5′H)-thione from powder synchrotron X-ray diffraction data
Avila, Edward E.
Mora, Asiloe J.
Delgado, Gerzon E.
Contreras, Ricardo R.
Fitch, Andrew N.
Brunelli, Michela
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 2008, 64 : 217 - 222
[35] ANTICANCER AGENT DEVELOPMENT .5. X-RAY STRUCTURE AND H-1-NMR SPECTRAL-ANALYSIS OF (1-ALPHA,2-ALPHA,5-ALPHA,6-ALPHA)-2,6-BIS(3,4-METHYLENEDIOXYPHENYL)-3,7-DIOXABICYCLO[3.3.0]OCTANE-4,8-DIONE
PETERSON, JR
PETERSON, S
BAKER, JK
ROGERS, RD
JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH, 1990, 20 (04): : 327 - 333
[36] SYNTHESIS AND REACTIVITY OF 6-CARBAMOYL-5-PHENYL-2,3,5,6-TETRAHYDRO-1H-1,4-ETHANOBENZO[F]QUINOLINE - X-RAY MOLECULAR-STRUCTURE OF (4AR-ASTERISK,5S-ASTERISK,6R-ASTERISK,10BR-ASTERISK)-5-PHENYL-2,3,4A,5,6,10B-HEXAHYDRO-1H-1,4-ETHANOBENZO[F]QUINOLIN-6-YL ACETATE
BESIDSKY, Y
LUTHMAN, K
CLAESSON, A
CSOREGH, I
HACKSELL, U
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1995, (04): : 475 - 480
[37] Porphyrazines with annulated diazepine rings, 1 synthesis and characterization of tetrakis-2,3-(5,7-diphenyl-6H-1,4-diazepino)porphyrazine and its MgII, CuII, and ZnII complexes -: X-ray crystal structure of 2,3-dicyano-5,7-diphenyl-6H-1,4-diazepine
Donzello, MP
Ercolani, C
Stuzhin, PA
Chiesi-Villa, A
Rizzoli, C
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 1999, (11) : 2075 - 2084
[38] CONFORMATION OF THE NOOTROPIC AGENTS 1-(4-METHOXYBENZOYL)-5-OXO-2-PYRROLIDINEPROPANOIC ACID (CI-933) AND 4-HYDROXYMETHYL-1-BENZYL-PYRROLIDIN-2-ONE (WEB-1868) - X-RAY CRYSTAL-STRUCTURES, THEORETICAL MO CALCULATIONS (AM-1) AND 600 MHZ H-1-NMR SPECTRA
AMATO, ME
BANDOLI, G
DJEDAINI, F
DOLMELLA, A
GRASSI, A
PAPPALARDO, GC
JOURNAL OF MOLECULAR STRUCTURE, 1990, 222 (3-4) : 487 - 502
[39] SYNTHESIS OF 2,3,5,6-TETRAHYDRO-1H,4H,11CH-3A,6A,11B-TRIAZABENZ[DE] ANTHRACENE (5) AND X-RAY CRYSTAL-STRUCTURE DETERMINATIONS OF (5), HEXAHYDRO-1H,4H,7H,9BH-3A,6A,9A-TRIAZAPHENALENE (1), BENZO[B]-1,5,9-TRIAZADODECANE N,N',N''-TRITOSYLAMIDE, AND OF 1,5,9-TRIAZADODECANE N,N',N''-TRITOSYLAMIDE
BEDDOES, RL
EDWARDS, WD
JOULE, JA
MILLS, OS
STREET, JD
TETRAHEDRON, 1987, 43 (08) : 1903 - 1920
[40] MOLECULAR DETERMINANTS FOR DRUG RECEPTOR INTERACTIONS - SOLID-STATE STRUCTURE AND CONFORMATION OF THE COGNITION ACTIVATOR 3-PHENOXYPYRIDINE SULFATE C-13 X-RAY, TWO-DIMENSIONAL H-1-NMR AND C-13 NMR, AND THEORETICAL MO-MNDO STUDIES
BANDOLI, G
GRASSI, A
MONTONERI, E
PAPPALARDO, GC
PERLY, B
JOURNAL OF MOLECULAR STRUCTURE, 1988, 172 : 369 - 380

← 1 2 3 4 5 →