RAPID-DETERMINATION OF SPARTEINE AND ITS METABOLITES IN URINE

被引:2
|
作者
VENINGEROVA, M [1 ]
PRACHAR, V [1 ]
LUKACSOVA, M [1 ]
GLASA, J [1 ]
HOLOMAN, J [1 ]
机构
[1] POSTGRAD MED INST,DEPT CLIN PHARMACOL,CS-83302 BRATISLAVA,SLOVAKIA
来源
关键词
D O I
10.1016/0378-4347(93)80277-B
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method is presented for the isolation, separation and determination of sparteine and its metabolites in urine. The isolation is based on rapid extraction with dichloromethane and pentane in a glass separator. For the separation and determination, capillary gas chromatography with nitrogen-phosphorus detection was used. The recovery of the method ranged from 81.6% to 94.8%, and the limit of determination varied between 0.2 and 0.5 mu g ml(-1). For quantification, 17-ethylsparteine was used as the internal standard.
引用
收藏
页码:274 / 277
页数:4
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