VINYLCYCLOPROPANATION OF NORBORNADIENE, NORBORNENE, AND DISPIROHEPTADIENE BY METHYL-ESTERS OF 1-ALKYLCYCLOPROPENE-3-CARBOXYLIC ACIDS

被引：1

作者：

PROTOPOPOVA, MN

SHAPIRO, EA

NEFEDOV, OM

机构：

[1] N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow

来源：

BULLETIN OF THE ACADEMY OF SCIENCES OF THE USSR DIVISION OF CHEMICAL SCIENCE | 1990年 / 39卷 / 01期

关键词：

D O I：

10.1007/BF00963033

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Methyl esters of 1-alkylcyclopropene-3-carboxylic acids (I) in the presence of CuCl·P(OPh)3cyclopropanate the intracyclic norbornene double bonds of norbornene, norbornadiene, and dispiroheptadiene to give the corresponding vinylcyclopropane adducts in yields up to 80%. 3,5-Dioxo-4-oxatricyclo[5.2.1. 02,6]dec-8-ene and 5-acetyl-7-oxabicyclo[2.2.1]hept-2-ene, which are heteroanalogs of dicyclopentadiene and norbornene, are inert relative to (I). © 1990 Plenum Publishing Corporation.

引用

页码：197 / 199

页数：3

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