SYNTHESIS, NMR-SPECTRA AND X-RAY CRYSTAL-STRUCTURE OF THE TRINUCLEAR COMPLEX [CH3C(CH2SPTH(PPH(3)))(3)].CH2CL2

被引：11

作者：

GHILARDI, CA ^{[1
]}

MIDOLLINI, S ^{[1
]}

ORLANDINI, A ^{[1
]}

SCAPACCI, G ^{[1
]}

VACCA, A ^{[1
]}

机构：

[1] CNR,IST STUDIO STEREOCHIM & ENERGET COMPOSTI COORDINA,I-50132 FLORENCE,ITALY

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1993年 / 461卷 / 1-2期

关键词：

D O I：

10.1016/0022-328X(93)83300-K

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The trinuclear hydride platinum complex [CH3C{CH2SPtH(PPh(3))}(3)] has been synthesized by oxidative addition of CH3C(CH2SH)(3) to [(PPh(3))(2)Pt(C2H4)] and it has been characterized by X-ray diffraction studies and multinuclear NMR spectroscopy.

引用

页码：C4 / C6

页数：3

共 50 条

[41] COORDINATION CHEMISTRY OF TRIPODAL TRIISOCYANIDE LIGANDS - SYNTHESIS OF COMPLEXES OF TYPE CH3C[CH2NC-M(COX]3 (M=CR,W,X=5 OR M=FE,X=4) AND CRYSTAL-STRUCTURE OF CH3C[CH2NC-W(CO)5]3
HAHN, FE
TAMM, M
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1991, 410 (01) : C9 - C12
[42] Reactions of Diethylaminodimethylaluminum Dimer with the Tripodal Ligands CH3C-(CH2NH2)2(CH2OH) and CH3C(CH2NH2)-(CH2OH)(CH2SPh): Crystal Structure of [AlMe2]3Al[CH3C(CH2NH)2(CH2O)$R B@2
Li, M.-D.
Chang, C.-C.
Chiang, M. Y.
Liu, S.-T.
Inorganic Chemistry, 37 (07):
[43] Synthesis and NMR spectroscopy of [PtH3(triphos)](+) and [Pt(AuPPh3)(3)(triphos)](+) - Crystal structure of [Pt(AuPPh3)(3)(triphos)](+) (triphos = CH3C(CH2PPh2)(3))
Peter, M
Wachtler, H
EllmererMuller, E
Ongania, KH
Wurst, K
Peringer, P
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1997, 542 (02) : 227 - 233
[44] SYNTHESIS, NMR-SPECTRA, AND CRYSTAL-STRUCTURE OF TRIPHENYLPHOSPHONIUM CYCLOBUTYLIDE, (C6H5)3P=C[CH2]3
SCHMIDBAUR, H
SCHIER, A
NEUGEBAUER, D
CHEMISCHE BERICHTE-RECUEIL, 1983, 116 (06): : 2173 - 2179
[45] RHENIUM POLYHYDRIDE COMPLEXES THAT CONTAIN THE TRIPODAL PHOSPHINE CH3C(CH2PPH2)3 (TRIPHOS)
COSTELLO, MT
FANWICK, PE
GREEN, MA
WALTON, RA
INORGANIC CHEMISTRY, 1992, 31 (12) : 2359 - 2365
[46] ASYMMETRICAL MONOCATIONIC OR NEUTRAL GOLD(II) COMPLEXES - X-RAY CRYSTAL-STRUCTURE OF [(C6F5)AU(CH2PPH2CH2)2AUPPH3]CLO4.0.5CH2CL2
LAGUNA, A
LAGUNA, M
JIMENEZ, J
LAHOZ, FJ
OLMOS, E
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1992, 435 (1-2) : 235 - 247
[47] INTERMOLECULAR POTENTIALS FOR CH4, CH3F, CHF3, CH3CL, CH2CL2, CH3CN AND CO2
BOHM, HJ
AHLRICHS, R
SCHARF, P
SCHIFFER, H
JOURNAL OF CHEMICAL PHYSICS, 1984, 81 (03): : 1389 - 1395
[48] RATE CONSTANTS FOR THE REACTIONS OF OH WITH CH3CL, CH2CL2, CHCL3, AND CH3BR
HSU, KJ
DEMORE, WB
GEOPHYSICAL RESEARCH LETTERS, 1994, 21 (09) : 805 - 808
[49] THE CRYSTAL-STRUCTURE OF MOO2CL2[(CH3OCH2CH2)2P(O)CH2CH2P(O)(CH2CH2OCH3)2]
HERBOWSKI, A
LIS, T
DEUTSCH, EA
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1993, 460 (01) : 25 - 30
[50] Kinetics and mechanism of the reactions of 2,3-butadione with F and Cl atoms, UV absorption spectra of CH3C(O)C(O)CH2• and CH3C(O)C(O)CH2O2• radicals, and atmospheric fate of CH3C(O)C(O)CH2O• radicals
Christensen, LK
Sehested, J
Nielsen, OJ
Wallington, TJ
Guschin, A
Hurley, MD
JOURNAL OF PHYSICAL CHEMISTRY A, 1998, 102 (45): : 8913 - 8923

← 1 2 3 4 5 →