ANALYSIS OF H-2, F2 AND O2 IN MIXTURES WITH HE AND HF

被引:4
|
作者
FOON, R [1 ]
REID, GP [1 ]
机构
[1] UNIV NEW S WALES,SCH CHEM,KENSINGTON 2033,NEW S WALES,AUSTRALIA
关键词
FLUORINE - Chromatographic Analysis - OXYGEN - Chromatographic Analysis;
D O I
10.1093/chromsci/14.9.421
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
A direct injection gas chromatography system with a Teflon column of chlorofluorocarbon oil supported on Kel-F immersed in liquid nitrogen has been used to analyze mixtures of H//2 and F//2 containing He and HF sampled from a flow reactor. Oxygen at trace levels in these mixtures was determined with a precolumn of molecular sieve 5A followed by one of activated charcoal. Teflon tubing was excluded from the system for this analysis because of its permeability to air.
引用
收藏
页码:421 / 422
页数:2
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