N-(4,6-DIMETHYLPYRID-2-YL)-2-(3-NITROPHENYL)ACETAMIDE

被引：1
|
作者：
RODIER, N [1 ]
ROBERT, JM [1 ]
ROBERTPIESSARD, S [1 ]
LEBAUT, G [1 ]
机构：
[1] FAC PHARM NANTES,CHIM THERAPEUT LAB,F-44035 NANTES,FRANCE
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷
关键词：
D O I：
10.1107/S010827019200859X
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The molecule of the title compound can be regarded as being composed of two parts, an N-(4,6-dimethylpyrid-2-yl)acetamide group and a 3-methyl-nitrobenzene group, which share the C(9) atom. The two parts are approximately planar. The least-squares planes through the pyridyl and phenyl rings make an angle of 64.5 (1)-degrees. An intramolecular hydrogen bond [C(3)-H(3)...O(18): 2.870 (4) angstrom, 114 (3)-degrees] forms a pseudo ring and contributes to the planarity of the N-(4,6-dimethylpyrid-2-yl)acetamide group. The molecules are linked together by. the N(7)-H(7)...O(18i) hydrogen bond [(i) x, 1/2 - y, 1/2 + z; 2.859 (3) angstrom, 170 (3)-degrees]. They form two chains parallel to the c axis and related by a centre of symmetry.
引用
收藏
页码：154 / 156
页数：3
相关论文
共 50 条
  • [21] 2-(4-Bromophenyl)-N-(5-methylpyridin-2-yl)acetamide
    Fun, Hoong-Kun
    Ooi, Chin Wei
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02526 - +
  • [22] N-(3-Chloro-4-fluorophenyl)-2-(naphthalen-1-yl)acetamide
    Praveen, A. S.
    Jasinski, Jerry P.
    Golen, James A.
    Narayana, B.
    Yathirajan, H. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1826 - U1869
  • [23] N-(3-nitrophenyl) methanesulfonamide
    Gowda, B. Thimme
    Foro, Sabine
    Fuess, Hartmut
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2337 - U664
  • [24] N-(3-nitrophenyl)maleimide
    Moreno-Fuquen, Rodolfo
    Valencia, Hoover
    Pardo, Zulay Diney
    D'Vries, Richard
    Kennedy, Alan R.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2734 - O2735
  • [25] N-(4-Chlorophenyl)-2-(naphthalen-1-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02463 - +
  • [26] N-(4-Bromophenyl)-2-(naphthalen-1-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Narayana, B.
    Nayak, Prakash S.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2926 - U415
  • [27] N-[2-(4,6-dimethoxypyrimidin-2-yl-carbonyl)phenyl]benzamide
    Li, Yuanxiang
    Huang, Gang
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4667 - U4659
  • [28] N-(3-nitrophenyl)-N′-pivaloylthiourea
    Yusof, M. Sukeri M.
    Muharam, Siti Hajar
    Kassim, M. B.
    Yamin, Bohari M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1137 - U2690
  • [29] 2-(3-Nitrophenyl)-2-oxazoline
    Decken, Andreas
    Botelho, Laura
    Sadowy, Amber L.
    Yadav, Paras N.
    Gossage, Robert A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O5414 - O5416
  • [30] 2-(3-Nitrophenyl)-4-oxo-4-phenylbutanenitrile
    Yang, Jingya
    Zhou, Hongyan
    Li, Zheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1610 - U2225
12345