Syntheses and Characterization of 2D and 3D Organotin Polymers with Phenylsuccinic Acid and Trimethyltin Chloride Under Different Conditions

被引：0
|
作者：
Rufen Zhang
Yun Ren
Qingfeng Wang
Chunlin Ma
机构：
[1] Liaocheng University,Department of Chemistry
[2] Taishan University,undefined
来源：
Journal of Inorganic and Organometallic Polymers and Materials | 2010年 / 20卷
关键词：
Trimethyltin chloride; Phenylsuccinic acid; Crystal structures; Polymers; Chiral space group;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Two types of di- and trimethyltin(IV) polymers [(Me2Sn)4O2(C10H8O4)4]n1 and [(Me3Sn)2(C10H8O4)]n·DMF 2 have been synthesized by the reaction of trimethyltin chloride with (±)-phenylsuccinic acid under two different experimental conditions. Both of the complexes are characterized by elemental analysis, IR, NMR (1H, 13C, 119Sn) spectroscopy and X-ray crystallographic diffraction analysis. The structural analyses show that complex 1 is a two-dimensional corrugated sheet polymer consisting of dimeric tetraorganodistannoxane units and bridging ligands. Complex 2 is a 3D corrugated polymer in which the deprotoned acid occurs as a tetradentate ligand and is bonded by the four oxygen atoms. It is worth noting that the X-ray diffraction study reveals that complex 2 crystallizes in the orthorhombic space group P212121, which is chiral space group.
引用
收藏
页码：399 / 404
页数：5
相关论文
共 50 条
  • [31] Anion-Assisted Structural Variation of Cadmium Coordination Polymers: From 2D → 3D Inclined Polycatenation to 2D → 3D Polythreading
    Xu, Bo
    Lue, Jian
    Cao, Rong
    CRYSTAL GROWTH & DESIGN, 2009, 9 (07) : 3003 - 3005
  • [32] Syntheses and structures of 1D, 2D, 3D cadmium(II) coordination polymers with oxalate and aromatic co-ligands
    Xia, SQ
    Hu, SM
    Dai, JC
    Wu, XT
    Fu, ZY
    Zhang, HJ
    Du, WX
    POLYHEDRON, 2004, 23 (06) : 1003 - 1009
  • [33] Factors Affecting the Behaviour of Retaining Structures with Prestressed Anchorages Under 2D and 3D Conditions
    Papadopoulou, Konstantina
    Sofianos, Alexandros
    GEOTECHNICAL AND GEOLOGICAL ENGINEERING, 2016, 34 (06) : 1877 - 1887
  • [34] 2D and 3D interlaminar fracture assessment under mixed-mode loading conditions
    Nikbakht, M.
    Choupani, N.
    Hosseini, S. R.
    MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 516 (1-2): : 162 - 168
  • [35] A series of 1D, 2D and 3D coordination polymers based on a 5-(benzonic-4-ylmethoxy)isophthalic acid: syntheses, structures and photoluminescence
    Liu, Ying-Ying
    Li, Jing
    Ma, Jian-Fang
    Ma, Ji-Cheng
    Yang, Jin
    CRYSTENGCOMM, 2012, 14 (01): : 169 - 177
  • [36] Physicists prove that 2D and 3D liquids are fundamentally different
    不详
    AMERICAN CERAMIC SOCIETY BULLETIN, 2020, 99 (02): : 18 - 18
  • [37] Multivalent 1D, 2D and 3D polymers as potent inhibitors for pathogens
    Haag, Rainer
    Ziem, Benjamin
    Bhatia, Sumati
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2016, 252
  • [38] 21/2D or 3D?
    Roth, S
    Küster, B
    Sura, H
    KUNSTSTOFFE-PLAST EUROPE, 2004, 94 (07): : 65 - 67
  • [39] 2D and 3D on demand
    Philippi, Anne
    F & M; Feinwerktechnik, Mikrotechnik, Messtechnik, 1998, 106 (06): : 412 - 414
  • [40] From 2D to 3D
    Steven De Feyter
    Nature Chemistry, 2011, 3 (1) : 14 - 15
12345